1-(3-Cyano-phen-yl)-3-(2-furo-yl)thio-urea.
作者信息
Theodoro Jahyr E, Mascarenhas Yvonne, Ellena Javier, Estévez-Hernández Osvaldo, Duque Julio
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2008 Jun 7;64(Pt 7):o1193. doi: 10.1107/S1600536808016012.
Abstract
The title compound, C(13)H(9)N(3)O(2)S, was synthesized from furoyl isothio-cyanate and 3-amino-benzonitrile in dry acetone. The thio-urea group is in the thio-amide form. The thio-urea fragment makes dihedral angles of 3.91 (16) and 37.83 (12)° with the ketofuran group and the benzene ring, respectively. The mol-ecular geometry is stabilized by N-H⋯O hydrogen bonds. In the crystal structure, centrosymmetrically related mol-ecules are linked by two inter-molecular N-H⋯S hydrogen bonds to form dimers.
摘要
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