Penteado Roberta Alves Pinto Moura, Tonholo Josealdo, Júnior José Ginaldo, Silva Milton Fernando de Andrade, Queiroz Celso da Silva, Cavalli Vanessa, Rego Marcos Augusto do, Liporoni Priscila Christiane Suzy
Federal University of Alagoas, Maceio, Brazil.
J Contemp Dent Pract. 2010 Dec 1;11(6):E017-24.
This study evaluated the surface roughness patterns of two resin-based composite restorative materials, a microhybrid (Filtek Z250, 3M ESPE) and a nanofilled (Filtek Supreme, 3M ESPE), subjected to a regimen that simulated dynamic pH-cycling and toothbrushing.
Twelve standardized cylindrical specimens of each resin-based composite material were prepared, finished, and mechanically polished. The experimental units were submitted to a pH-cycling regimen followed by 50,000 toothbrushing cycles, after which the surface roughness was measured using an atomic force microscope (AFM). AFM surface roughness was evaluated at three intervals: (1) immediately after specimen preparation (baseline), (2) after pH-cycling, and (3) after simulated toothbrushing. The results were then analyzed using a split-plot design and followed by linear regression and a Tukey's test at a significance level of p<0.05.
The results obtained indicated that simulated toothbrushing provoked a remarkable increase in surface roughness for both types of composite resins tested (p=0.0031). However, pH-cycling did not alter the surface of the composite under the conditions of this experiment.
Based on the results obtained, it was concluded that simulated toothbrushing was capable of increasing the surface roughness of the microhybrid (Filtek Z250) and the nanofilled (Filtek Supreme) composites tested.
Surface roughness of nanofilled and microhybrid composites is significantly increased after toothbrushing, although pH-cycling, as tested in this study, does not appear to affect the morphology of either composite material.
本研究评估了两种树脂基复合修复材料——一种微混合材料(Filtek Z250,3M ESPE公司)和一种纳米填料材料(Filtek Supreme,3M ESPE公司),在模拟动态pH循环和刷牙的方案下的表面粗糙度模式。
制备、修整并机械抛光每种树脂基复合材料的12个标准化圆柱形试件。将实验单元进行pH循环方案,随后进行50000次刷牙循环,之后使用原子力显微镜(AFM)测量表面粗糙度。在三个时间点评估AFM表面粗糙度:(1)试件制备后立即(基线),(2)pH循环后,以及(3)模拟刷牙后。然后使用裂区设计分析结果,接着进行线性回归和Tukey检验,显著性水平为p<0.05。
所得结果表明,对于所测试的两种复合树脂,模拟刷牙均导致表面粗糙度显著增加(p=0.0031)。然而,在本实验条件下,pH循环并未改变复合材料的表面。
基于所得结果,得出结论:模拟刷牙能够增加所测试的微混合材料(Filtek Z250)和纳米填料材料(Filtek Supreme)复合材料的表面粗糙度。
纳米填料和微混合复合材料在刷牙后的表面粗糙度显著增加,尽管如本研究中所测试的,pH循环似乎并未影响任何一种复合材料的形态。