A.A. Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Moscow, Russia.
J Biomater Appl. 2012 May;26(8):1051-68. doi: 10.1177/0885328210390403. Epub 2011 Jan 27.
In this study, the phase development in the cement system α-TCP-OCP with phosphoric acid as a setting liquid was studied. The most promising formulation of α-TCP (60 wt%) and OCP (40 wt%) is proposed. This cement has the following characteristics: setting time 10 min, pH = 6.7, the compressive strength about 30 MPa, and high dissolution rate in an isotonic solution; the final wt% composition of α-TCP/DCPD/HA/OCP equals 27/38/20/15. Energy dispersive X-ray diffraction techniques were used for in situ monitoring of the processes taking place in the cement in real time.
在这项研究中,研究了以磷酸为凝固液的 α-TCP-OCP 水泥体系中的相发展。提出了最有前途的 α-TCP(60wt%)和 OCP(40wt%)配方。这种水泥具有以下特点:凝固时间 10 分钟,pH 值=6.7,抗压强度约 30MPa,在等渗溶液中具有较高的溶解速率;最终 wt%的 α-TCP/DCPD/HA/OCP 组成比例为 27/38/20/15。使用能量色散 X 射线衍射技术实时原位监测水泥中发生的过程。