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利用小型选区光阑估计透射电子显微镜中入射束的波场。

Estimation of wave fields of incident beams in a transmission electron microscope by using a small selected-area aperture.

作者信息

Morishita Shigeyuki, Yamasaki Jun, Tanaka Nobuo

机构信息

Department of Crystalline Materials Science, Nagoya University, Furo-cho, Nagoya 464-8603, Japan.

出版信息

J Electron Microsc (Tokyo). 2011;60(2):101-8. doi: 10.1093/jmicro/dfr002. Epub 2011 Feb 13.

Abstract

The direction of an electron beam in a nanometer-sized area is measured directly by utilizing a selected-area aperture. By the measurements at several areas in a beam, the wavefront curvature and thus the defocus value of the beam are detected. From the defocus value, the wave field at the specimen plane is also reproduced in consideration of the influences of the condenser aperture and spherical aberration of the illumination lens. The result shows that phase deviation of 2π is caused only at about 10 nm apart from the beam center in a beam with a typical diameter for high-resolution transmission electron microscopy. Based on the defocus value, the convergence angle of the beam is also estimated to be about 6 mrad without being influenced by the partial coherence, that is, independently of the type of the electron gun. Measuring the defocus values for only two beam diameters enables us to determine geometrical parameters peculiar to the illumination system, based on which wave fields of any beam diameters by any condenser aperture sizes can be estimated. The technique proposed in this paper is effective in evaluating the influence of wavefront curvature of incident beams on various kinds of precise measurements conducted in transmission electron microscopes.

摘要

利用选区光阑直接测量纳米尺寸区域内电子束的方向。通过对电子束中多个区域的测量,检测波前曲率,进而检测电子束的散焦值。考虑到聚光镜光阑和照明透镜球差的影响,根据散焦值还可再现样品平面处的波场。结果表明,在具有高分辨率透射电子显微镜典型直径的电子束中,仅在距束中心约10纳米处会产生2π的相位偏差。基于散焦值,还可估计电子束的会聚角约为6毫弧度,且不受部分相干性的影响,即与电子枪的类型无关。仅测量两个束直径的散焦值,就能确定照明系统特有的几何参数,据此可估计任何聚光镜光阑尺寸下任何束直径的波场。本文提出的技术对于评估入射电子束波前曲率对透射电子显微镜中各种精确测量的影响是有效的。

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