Laboratory for Biomaterials, Department of Materials Science and Engineering, Indian Institute of Technology, Kanpur, India.
J Biomater Appl. 2012 Jul;27(1):67-78. doi: 10.1177/0885328210393292. Epub 2011 Feb 22.
Herein, the results of systematic mechanical property measurements of pressureless sintered calcium phosphate (CaP)-mullite composites are discussed. Our experimental results demonstrated how the mullite addition (upto 30 wt%) influenced hardness, elastic modulus, strength and toughness properties of the composites. In assessing each of these fundamental material properties, either a range of load or a number of complimentary techniques were used to obtain reliable measure of mechanical properties. Importantly, the results of single edge V notch beam measurements revealed that a reliable toughness value of 1.5 MPa m(0.5) could be obtained in composites containing 20 or 30 wt% mullite. Our results clearly illustrated that a combination of elastic modulus (80 GPa), compressive strength of more than 350 MPa, three-point flexural strength of 70-80 MPa, hardness of 4-5 GPa were achievable with the investigated composites. Such a combination of material properties, in addition to modest toughness property appeared to indicate that CaP-mullite composites could be used as a biomaterial for hard tissue replacement.
本文讨论了无压烧结磷酸钙(CaP)-莫来石复合材料系统力学性能测量的结果。我们的实验结果表明,莫来石的添加(高达 30wt%)如何影响复合材料的硬度、弹性模量、强度和韧性。在评估这些基本材料性能中的每一个时,要么使用一系列载荷,要么使用几种互补技术来获得可靠的力学性能测量值。重要的是,单边 V 型缺口梁测量的结果表明,在含有 20 或 30wt%莫来石的复合材料中可以获得可靠的韧性值约为 1.5MPa·m(0.5)。我们的结果清楚地表明,研究复合材料可以实现的弹性模量(约 80GPa)、抗压强度超过 350MPa、三点弯曲强度为 70-80MPa、硬度为 4-5GPa 的组合。这种材料性能的组合,加上适度的韧性特性,似乎表明 CaP-莫来石复合材料可用作硬组织替代的生物材料。