Sakai M
First Department of Prosthodontics, Asahi University, Graduate School of Dentistry.
Gifu Shika Gakkai Zasshi. 1990 Jun;17(1):280-309.
Pure titanium produced by a commercial pure titanium casting system was studied for use as a cast plate for clinical application. The mechanical properties, elemental analysis, castability, adaptability of pure titanium and adhesion to denture base resin were investigated. The interfacial zone of the pure titanium castings was composed of a layered structure obtained by reaction with phosphate bonded Al2O3/SiO2 investment material. Vicher's hardness at 100 microns thick from the surface was higher than that in the inner part by oxidation. Cast pure titanium showed tensile strength, elongation and hardness close to those of the type III or IV dental gold alloy. The castability of pure titanium was lower than that of Co-Cr alloy and pure titanium castings also had large casting defects. Adaptability between pure titanium cast plate and the working model was satisfactory when reversible hydrocolloid impression material was used with heating-bath treatment in the refractory model. The tensile and compressive shear bonding strength of pure titanium to heat-curing or self-curing resin were similar to that of the Co-Cr alloy, and surface treatment using a solution containing 2-vol% 3-methacryloxypropyltrimethoxysilane produced a higher bonding strength than non-treatment, MKV treatment and 4-META treatment. These findings suggest that pure titanium castings produced by this system have suitable mechanical properties, adaptability and adhesion to denture base resin, and is available for cast plate in clinical application.
研究了商用纯钛铸造系统生产的纯钛用作临床应用铸造板的情况。对纯钛的力学性能、元素分析、铸造性能、适应性以及与义齿基托树脂的附着力进行了研究。纯钛铸件的界面区由与磷酸盐粘结的Al2O3/SiO2包埋材料反应形成的层状结构组成。表面100微米厚处的维氏硬度因氧化而高于内部。铸造纯钛的拉伸强度、伸长率和硬度接近III型或IV型牙科金合金。纯钛的铸造性能低于钴铬合金,纯钛铸件也有较大的铸造缺陷。当在耐火模型中使用可逆水胶体印模材料并进行加热浴处理时,纯钛铸造板与工作模型之间的适应性令人满意。纯钛与热固化或自固化树脂的拉伸和压缩剪切粘结强度与钴铬合金相似,使用含2体积% 3-甲基丙烯酰氧基丙基三甲氧基硅烷的溶液进行表面处理比未处理、MKV处理和4-META处理产生更高的粘结强度。这些发现表明,该系统生产的纯钛铸件具有合适的力学性能、适应性以及与义齿基托树脂的附着力,可用于临床应用中的铸造板。