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[不同炮制方法对半夏中甾醇类成分的影响]

[Effect of original processing method on sterol compounds of rhizoma pinelliae].

作者信息

Chen Qian, Chen Ke-Li, Yang Min, Yang Cheng-Xiong

机构信息

Key laboratory of Traditional Chinese Medicine Resource and Compound Prescription, Hubei University of Traditional Chinese Medicine, Wuhan 430065, China.

出版信息

Zhong Yao Cai. 2010 Nov;33(11):1701-3.

Abstract

OBJECTIVE

Investigate the effect of different processing methods on the quality of Rhizoma Pinelliae.

METHODS

The sterol compounds from different Rhizoma Pinelliae samples processed with different drying methods were analysed by GC.

RESULTS

The fingerprints of five specific steroid components are very stable in those samples of Rhizoma Pinelliae which were first dried 2 h at 70 degrees C then baked at low temperature or by repeated drying at low-temperature, and the the five peaks from each sample have high similarity. But the samples dried without a proper treatment on higher temperature or with a halfway dryness at low-temperature showed a reduced peak height of steroid to varying degrees and some peaks were hardly detected.

CONCLUSION

It is conducive to the preservation and stability of stroids of Pinellia ternata that to being Dried at proper high temperature such as at 70 degrees C for 2 h first then fully dried at low temperature.

摘要

目的

考察不同炮制方法对半夏质量的影响。

方法

采用气相色谱法分析不同干燥方法炮制的半夏样品中的甾醇类化合物。

结果

先于70℃干燥2小时,再低温烘烤或反复低温干燥的半夏样品中,5种特定甾体成分的指纹图谱非常稳定,各样品的5个峰相似度高。但未经适当高温处理或低温半干处理的样品,甾体峰高不同程度降低,部分峰难以检出。

结论

先于70℃等适当高温干燥2小时,再低温充分干燥,有利于半夏甾体成分的保存和稳定。

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