• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利：CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法，用中文像聊天一样搜索，搜遍4000万医学文献。AI智能推荐，让科研检索更轻松。

立即免费搜索

文件翻译

保留排版，准确专业，支持PDF/Word/PPT等文件格式，支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述，25分钟生成高质量综述，智能提取关键信息，辅助科研写作。

立即免费体验

[顶空气相色谱-质谱联用快速测定莪术中的挥发性成分]

[Fast determination of volatile components in rhizoma curcuma by headspace gas chromatography-mass spectrometry].

作者信息

Lv Di-Ya, Lou Zi-Yang, Li Ling, Cao Yan, Zhang Hai, Chai Yi-Feng

机构信息

School of Pharmacy, Second Military Medical University, Shanghai 200433, China.

出版信息

Zhong Yao Cai. 2010 Nov;33(11):1732-6.

PMID:21434435
Abstract

OBJECTIVE

To analyze the chemical constituents of essential oil extracted from Rhizoma Curcumae.

METHODS

Headspace-GC/MS was employed to prepare essential oil from rhizome curcuma, with TR-5 quartz capillary column, extraction temperature 90 degrees C, hold 30 min, injection volume 1.5 mL.

CONCLUSION

A rapid, simple and reliable method using HS-GC/MS was developed to analyze 79 volatile components, which can be an alternative for quality control for TCMs such as Rhizome Curcuma.

摘要

目的

分析莪术挥发油的化学成分。

方法

采用顶空-气相色谱/质谱联用技术从莪术根茎中制备挥发油，使用TR-5石英毛细管柱，萃取温度90℃，保持30分钟，进样量1.5毫升。

结论

建立了一种快速、简便、可靠的顶空-气相色谱/质谱联用方法来分析79种挥发性成分，可作为莪术等中药质量控制的替代方法。

相似文献

1
[Fast determination of volatile components in rhizoma curcuma by headspace gas chromatography-mass spectrometry].[顶空气相色谱-质谱联用快速测定莪术中的挥发性成分]
Zhong Yao Cai. 2010 Nov;33(11):1732-6.
2
[Comparisons of volatile components in different parts of three species of Rhizoma Curcumae].[三种姜黄不同部位挥发成分的比较]
Zhong Yao Cai. 2009 Oct;32(10):1551-3.
3
[Analysis of volatile oil in pre and post processed pieces of Eriobotrya japonica by GC-MS].[气相色谱-质谱联用分析枇杷炮制前后饮片的挥发油]
Zhong Yao Cai. 2008 Nov;31(11):1625-6.
4
[Naphtha analysis of different processed products of Rhizoma Curcumae from Guangxi by GC-MS].[广西莪术不同炮制品的石脑油成分的气相色谱-质谱联用分析]
Zhong Yao Cai. 2009 Mar;32(3):339-42.
5
[Analysis of volatile oil from Gerbera piloselloides by GC-MS].[假地胆草挥发油的气相色谱-质谱联用分析]
Zhong Yao Cai. 2013 Jun;36(6):944-5.
6
[Analysis of compositions of the essential oil from Curcuma aromatica by gas chromatography-mass spectrometry].[气相色谱-质谱联用分析莪术挥发油的成分]
Zhong Yao Cai. 2012 Jul;35(7):1102-4.
7
[Comparison of volatile oil chromatographic fingerprints of rhizoma curcumae longae and rhizoma wenyujin concisum].[莪术与温莪术挥发油色谱指纹图谱的比较]
Zhong Yao Cai. 2006 Nov;29(11):1179-82.
8
[Study on ingredients of essential oils of Curcuma wenyujin extracted by supercritical-CO2 fluid extraction and steam distillation].[超临界CO₂流体萃取法与水蒸气蒸馏法提取温郁金挥发油成分的研究]
Zhongguo Zhong Yao Za Zhi. 2006 Sep;31(17):1445-6.
9
[Analysis of the volatile oils chemical constituents of roots of Actinidia deliciosa].美味猕猴桃根挥发油化学成分分析
Zhong Yao Cai. 2008 May;31(5):677-8.
10
[Study on preparation of beta-cyclodextrin inclusion volatile oil from Rhizoma Curcumae].[莪术β-环糊精包合物挥发油的制备研究]
Zhong Yao Cai. 2004 Nov;27(11):866-9.