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1-氯-4-（3,4-二氯苯基）-3,4-二氢萘-2-甲醛

1-Chloro-4-(3,4-dichloro-phen-yl)-3,4-dihydro-naphthalene-2-carbaldehyde.

作者信息

Devarajegowda H C, Nagendra P, Jeyaseelan S, Chidananda N, Poojary Boja

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 Jan 15;67(Pt 2):o378. doi: 10.1107/S160053681100105X.

DOI:10.1107/S160053681100105X
PMID:21523055
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3051754/
Abstract

The title compound, C(17)H(11)Cl(3)O, was synthesized via the Vilsmeier-Haack reaction. The dihydro-naphthalene ring system is non-planar, the dihedral angle between the two fused rings being 10.87 (13)°; it forms a dihedral angle of 81.45 (10)° with the dichloro-phenyl ring. The crystal structure features inter-molecular C-H⋯O hydrogen bonds.

摘要

标题化合物C(17)H(11)Cl(3)O通过Vilsmeier-Haack反应合成。二氢萘环系是非平面的，两个稠合环之间的二面角为10.87 (13)°；它与二氯苯基环形成的二面角为81.45 (10)°。晶体结构具有分子间C-H⋯O氢键。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b92b/3051754/7f78c3ca2f6f/e-67-0o378-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b92b/3051754/1e3e2d8bb35c/e-67-0o378-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b92b/3051754/7f78c3ca2f6f/e-67-0o378-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b92b/3051754/1e3e2d8bb35c/e-67-0o378-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b92b/3051754/7f78c3ca2f6f/e-67-0o378-fig2.jpg

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本文引用的文献

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A short history of SHELX.SHELX简史。
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