Kim Nam-Ho, Hwang In-Chul, Ha Kwang
Acta Crystallogr Sect E Struct Rep Online. 2009 Aug 12;65(Pt 9):o2128. doi: 10.1107/S1600536809031110.
In the title compound, C(10)H(26)N(4) (2+)·2Cl(-)·0.5H(2)O, the cyclam (1,4,8,11-tetra-azacyclo-tetra-decane) dication adopts an endodentate conformation which my be inflenced by intra-molecular N-H⋯N hydrogen bonding. In the crystal structure, the components are linked by N-H⋯Cl and O-H⋯Cl hydrogen bonds into chains along [100]. The water molecule is disordered over two sites in a 50:50 ratio.
在标题化合物C(10)H(26)N(4)(2+)·2Cl(-)·0.5H(2)O中，环胺（1,4,8,11-四氮杂环十四烷）双阳离子采取内齿构象，这可能受分子内N-H⋯N氢键的影响。在晶体结构中，各组分通过N-H⋯Cl和O-H⋯Cl氢键沿[100]方向连接成链。水分子在两个位置上无序分布，比例为50:50。
