Jiang Xue-Yue, Feng Xiao-Jun, Yang Song, Xu Hua-Jie, Hao Ling-Yun
Acta Crystallogr Sect E Struct Rep Online. 2009 Aug 19;65(Pt 9):o2189. doi: 10.1107/S160053680903181X.
The title mol-ecule, C(14)H(10)N(4)O(6), crystallizes with one half-mol-ecule in the asymmetric unit; the mid-point of the N-N bond lies on an inversion centre. The nitro and amide groups are twisted with respect to the benzene ring, making dihedral angles of 14.6 (5) and 31.1 (5)°, respectively. In the crystal structure, mol-ecules are linked through N-H⋯O hydrogen bonding between the imino and carbonyl groups.
标题分子C(14)H(10)N(4)O(6)在不对称单元中以半个分子结晶;N-N键的中点位于一个对称中心上。硝基和酰胺基相对于苯环发生扭曲,二面角分别为14.6 (5)°和31.1 (5)°。在晶体结构中,分子通过亚氨基和羰基之间的N-H⋯O氢键相连。