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N,N'-双（4-氯苯基）萘-1,4-二甲酰胺 N,N-二甲基甲酰胺二溶剂化物

N,N'-Bis(4-chloro-phen-yl)naphthalene-1,4-dicarboxamide N,N-dimethyl-formamide disolvate.

作者信息

Jing Lin-Hai

机构信息

School of Chemistry and Chemical Engineering, China West Normal University, Nanchong 637002, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Sep 9;65(Pt 10):o2414. doi: 10.1107/S1600536809034394.

DOI:10.1107/S1600536809034394
PMID:21577873
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2970211/
Abstract

In the title compound, C(24)H(16)Cl(2)N(2)O(2)·2C(3)H(7)NO, the two C=O groups adopt an anti orientation. The two amide groups are twisted away from the naphthalene ring system by 59.10 (4) and 68.22 (4)°. The crystal packing is stabilized by N-H⋯O and C-H⋯O hydrogen bonds.

摘要

在标题化合物C(24)H(16)Cl(2)N(2)O(2)·2C(3)H(7)NO中，两个C=O基团呈反式取向。两个酰胺基团与萘环体系扭转的角度分别为59.10 (4)°和68.22 (4)°。晶体堆积通过N-H⋯O和C-H⋯O氢键得以稳定。

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本文引用的文献

1
N,N'-Bis(4-methyl-phen-yl)naphthalene-1,4-dicarboxamide N,N-dimethyl-acetamide disolvate.N,N'-双(4-甲基苯基)萘-1,4-二甲酰胺 N,N-二甲基乙酰胺溶剂化物
Acta Crystallogr Sect E Struct Rep Online. 2008 Nov 20;64(Pt 12):o2379. doi: 10.1107/S1600536808037422.
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A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
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N,N'-bis(2-methoxyphenyl)naphthalene-1,4-dicarboxamide.
Acta Crystallogr C. 2006 Sep;62(Pt 9):o561-2. doi: 10.1107/S0108270106026928. Epub 2006 Aug 11.