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A second monoclinic polymorph of N-cyclo-hexyl-N-ethyl-benzene-sulfonamide.

作者信息

Haider Zeeshan, Arshad Muhammad Nadeem, Zia-Ur-Rehman Muhammad, Khan Islam Ullah, Shafiq Muhammad

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Nov 18;65(Pt 12):o3107. doi: 10.1107/S160053680904762X.

Abstract

The crystal structure of the title compound, C(14)H(21)NO(2)S, is a polymorph of the structure reported by Khan et al. [Acta Cryst. (2009), E65, o2867] which is also monoclinic (space group P2(1)/c). The unit cell in the title structure is approximately half the volume of the previously reported polymorph and the asymmetric unit of the title compound contains one mol-ecule rather than two independent mol-ecules in the other polymorph. In the title mol-ecule, the cyclo-hexane ring is in the typical chair form. In the crystal structure, mol-ecules are linked via weak inter-molecular C-H⋯O inter-actions, forming a chain along the b-axis direction.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8df7/2972150/159c520266b0/e-65-o3107-fig1.jpg

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