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μ-Adipato-κO:O-bis-{[2,6-bis-(1H-benzimidazol-2-yl-κN)pyridine-κN](nitrato-κO)lead(II)}.

作者信息

Wei Lian-Qiang, Zeng Ming-Hua, Ng Seik Weng

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Dec 12;66(Pt 1):m56. doi: 10.1107/S1600536809052647.

DOI:10.1107/S1600536809052647
PMID:21579952
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2980214/
Abstract

The dinuclear title compound, [Pb(2)(C(6)H(8)O(4))(NO(3))(2)(C(19)H(13)N(5))(2)], lies with the mid-point of the butyl chain of the bridging adipate unit on a center of inversion. The Pb(II) ion is covalently bonded to the nitrate anion and is bonded to a carboxyl-ate group of the adipate unit by another covalent bond. The N-heterocycle functions in a chelating tridentate mode. The metal atom exists in a Ψ-octa-hedral coordination environment. When weaker Pb⋯O inter-actions are also considered, the geometry is a Ψ-tricapped trigonal prism in which the lone-pair electrons occupy one face of the trigonal prism. Adjacent mol-ecules are linked into a layer structure by N-H⋯O hydrogen bonds.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/43c0/2980214/6068fc3ee9ac/e-66-00m56-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/43c0/2980214/6160e6966e6a/e-66-00m56-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/43c0/2980214/6068fc3ee9ac/e-66-00m56-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/43c0/2980214/6160e6966e6a/e-66-00m56-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/43c0/2980214/6068fc3ee9ac/e-66-00m56-fig2.jpg

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