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N'-[(E)-1-(4-氯苯基)亚乙基]-2-[4-(2-甲基丙基)苯基]丙酰肼

N'-[(E)-1-(4-Chloro-phen-yl)ethyl-idene]-2-[4-(2-methyl-prop-yl)phen-yl]propano-hydrazide.

作者信息

Fun Hoong-Kun, Jebas Samuel Robinson, Sujith K V, Kalluraya B

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Dec 3;65(Pt 1):o17-8. doi: 10.1107/S1600536808039226.

DOI:10.1107/S1600536808039226
PMID:21581626
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2967938/
Abstract

The asymmetric unit of the title compound, C(21)H(25)ClN(2)O, contains four crystallographically independent mol-ecules, which differ mainly in the orientation of the isobutyl groups. The benzene rings are almost orthogonal to each other, forming dihedral angles of 87.40 (6), 88.69 (6), 84.88 (6) and 85.12 (6)° in the four mol-ecules. The crystal structure is stabilized by inter-molecular N-H⋯O and C-H⋯O hydrogen bonds, together with C-H⋯π inter-actions.

摘要

标题化合物C(21)H(25)ClN(2)O的不对称单元包含四个晶体学独立分子，它们主要在异丁基的取向上有所不同。苯环彼此几乎正交，在四个分子中形成的二面角分别为87.40 (6)°、88.69 (6)°、84.88 (6)°和85.12 (6)°。晶体结构通过分子间的N-H⋯O和C-H⋯O氢键以及C-H⋯π相互作用得以稳定。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6cf9/2967938/6e9775861732/e-65-00o17-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6cf9/2967938/d0285339e0a8/e-65-00o17-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6cf9/2967938/6e9775861732/e-65-00o17-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6cf9/2967938/d0285339e0a8/e-65-00o17-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6cf9/2967938/6e9775861732/e-65-00o17-fig2.jpg

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