（E）-N-[2-（3,5-二叔丁基-2-羟基苄叉氨基）环己基]-4-甲基苯磺酰胺
(E)-N-[2-(3,5-Di-tert-butyl-2-hydroxy-benzyl-ideneamino)cyclo-hexyl]-4-methyl-benzene-sulfonamide.
作者信息
Wu Jincai, Wang Lei, Pan Xiaobo, Yao Lihui
机构信息
College of Chemistry and Chemical Engineering, State Key Laboratory of Applied Organic Chemistry, Lanzhou University, Lanzhou 730000, People's Republic of China.
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2009 Jan 8;65(Pt 2):o255. doi: 10.1107/S1600536808043870.
In the crystal structure of the title compound, C(28)H(40)N(2)O(3)S, there are two mol-ecules per asymmetric unit; in each of these mol-ecules, the cyclo-hexyl rings adopt chair conformations. The dihedral angles between the benzene rings are 16.89 (9) and 34.11 (9)°. Each mol-ecule contains an intra-molecular O-H⋯N hydrogen bond, and inter-molecular N-H⋯O hydrogen bonds are also present. In both mol-ecules, the methyl groups of one tert-butyl group are disordered over two positions; the site-occupancy factors in both cases are ca 0.6 and 0.4.
在标题化合物C(28)H(40)N(2)O(3)S的晶体结构中，每个不对称单元有两个分子；在这些分子中的每一个中，环己基环均呈椅式构象。苯环之间的二面角分别为16.89 (9)°和34.11 (9)°。每个分子都包含一个分子内O-H⋯N氢键，并且也存在分子间N-H⋯O氢键。在两个分子中，一个叔丁基的甲基在两个位置上无序；两种情况下的占有率因子约为0.6和0.4。
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