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3-氨基甲酰基-4-甲氧基亚氨基-3-甲基哌啶-1-羧酸叔丁酯

tert-Butyl 3-carbamoyl-4-methoxy-imino-3-methyl-piperidine-1-carboxyl-ate.

作者信息

Chai Yun, Wan Zhi-Long, Guo Hui-Yuan, Liu Ming-Liang

机构信息

Institute of Medicinal Biotechnology, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jan 10;65(Pt 2):o282. doi: 10.1107/S1600536809000634.

DOI:10.1107/S1600536809000634
PMID:21581895
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2968237/
Abstract

In the title compound, C(13)H(23)N(3)O(4), the piperidine ring adopts a chair conformation. An intra-molecular N-H⋯O hydrogen bond is observed between the carbamoyl and carboxyl-ate groups. In the crystal structure, mol-ecules form inversion dimers linked by pairs of N-H⋯O hydrogen bonds.

摘要

在标题化合物C(13)H(23)N(3)O(4)中，哌啶环呈椅式构象。在氨基甲酰基和羧酸盐基团之间观察到分子内N-H⋯O氢键。在晶体结构中，分子通过成对的N-H⋯O氢键形成反演二聚体。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c4fa/2968237/23684255cc4a/e-65-0o282-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c4fa/2968237/fdbc72c5f694/e-65-0o282-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c4fa/2968237/23684255cc4a/e-65-0o282-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c4fa/2968237/fdbc72c5f694/e-65-0o282-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c4fa/2968237/23684255cc4a/e-65-0o282-fig2.jpg

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