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链状聚[[[二水合-铥(III)]-μ-6-羧基-烟酸根-μ-吡啶-2,5-二羧酸根]二水合物]

catena-Poly[[[diaqua-thulium(III)]-μ-6-carboxy-nicotinato-μ-pyridine-2,5-di-carboxyl-ato] dihydrate].

作者信息

Li Sheng, Chen Yue, He Hong-Mei, Ma Yuan-Fang

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Mar 19;65(Pt 4):m411. doi: 10.1107/S1600536809008836.

DOI:10.1107/S1600536809008836
PMID:21582354
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2968913/
Abstract

The title compound, {[Tm(C(7)H(3)NO(4))(C(7)H(4)NO(4))(H(2)O)(2)]·2H(2)O}(n), is isotypic with the analogous Tb(III) compound [Li et al. (2009 ▶). Acta Cryst. E65, m410]. All interatomic distances and angles and the hydrogen-bond geometries are very similar for the two structures. The refined Flack parameter of 0.49 (2) suggests inversion twinning.

摘要

标题化合物{[Tm(C₇H₃NO₄)(C₇H₄NO₄)(H₂O)₂]·2H₂O}ₙ与类似的Tb(III)化合物[Li等人(2009 ▶)。Acta Cryst. E65, m410]同型。两种结构的所有原子间距离、角度和氢键几何结构都非常相似。精修得到的Flack参数为0.49 (2)，表明存在倒易孪生。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ffd0/2968913/c88412c1f635/e-65-0m411-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ffd0/2968913/42843bb13990/e-65-0m411-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ffd0/2968913/999cd383e81d/e-65-0m411-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ffd0/2968913/c88412c1f635/e-65-0m411-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ffd0/2968913/42843bb13990/e-65-0m411-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ffd0/2968913/999cd383e81d/e-65-0m411-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ffd0/2968913/c88412c1f635/e-65-0m411-fig3.jpg

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本文引用的文献

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catena-Poly[[[diaqua-terbium(III)]-μ-6-carboxy-nicotinato-μ-pyridine-2,5-di-carboxyl-ato] dihydrate].链状聚[[[二水合铽(III)]-μ-6-羧基烟碱酸根-μ-吡啶-2,5-二羧酸根]二水合物]
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A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
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New lanthanide hybrid as clustered infinite nanotunnel with 3D Ln-O-Ln framework and (3,4)-connected net.
新型镧系杂化物，具有三维Ln-O-Ln框架和(3,4)连接网络的簇状无限纳米隧道。
Inorg Chem. 2007 Feb 19;46(4):1171-6. doi: 10.1021/ic0615271.