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N'-(3,4-二甲氧基-亚苄基)乙酰肼

N'-(3,4-Dimethoxy-benzyl-idene)aceto-hydrazide.

作者信息

Zhou Bao-Cheng, Lv Lu-Ping, Yu Wen-Bo, Li Wei-Wei, Hu Xian-Chao

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jul 25;65(Pt 8):o1964. doi: 10.1107/S1600536809028608.

DOI:10.1107/S1600536809028608
PMID:21583641
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2977217/
Abstract

The asymmetric unit of the title compound, C(11)H(14)N(2)O(3), contains two independent mol-ecules with close conformations; the C=N-N-C torsion angle is 176.4 (1)° in both mol-ecules. In the crystal, inter-molecular N-H⋯O and C-H⋯O hydrogen bonds link the mol-ecules into chains running along the [01] direction.

摘要

标题化合物C(11)H(14)N(2)O(3)的不对称单元包含两个构象相近的独立分子；两个分子中的C=N-N-C扭转角均为176.4 (1)°。在晶体中，分子间的N-H⋯O和C-H⋯O氢键将分子连接成沿[01]方向延伸的链。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/245d/2977217/dc46b03a7538/e-65-o1964-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/245d/2977217/dc46b03a7538/e-65-o1964-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/245d/2977217/dc46b03a7538/e-65-o1964-fig1.jpg

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A short history of SHELX.SHELX简史。
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