4-（4-溴苯基）-5-氧代-1,2,3,4,5,6,7,8-八氢喹唑啉-2-硫酮
4-(4-Bromo-phen-yl)-5-oxo-1,2,3,4,5,6,7,8-octa-hydro-quinazoline-2-thione.
作者信息
Xie Min, Deng Changquan, Zheng Jie, Zhu Yulin
机构信息
School of Chemistry and Environment, South China Normal University, Guangzhou 510006, People's Republic of China.
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2009 Jul 25;65(Pt 8):o1980. doi: 10.1107/S1600536809028761.
Abstract
The title compound, C(14)H(13)BrN(2)OS, was synthesized from the multicomponent reaction between thio-urea, 4-bromo-benzaldehyde and cyclo-hexane-1,3-dione. The crystal packing is stabilized by inter-molecular N-H⋯O, N-H⋯S, C-H⋯O and C-H⋯S hydrogen bonds. Br⋯O inter-actions [3.183 (3) Å] are also observed in the crystal structure.
摘要
标题化合物C(14)H(13)BrN(2)OS是由硫脲、4-溴苯甲醛和环己烷-1,3-二酮之间的多组分反应合成的。晶体堆积通过分子间的N-H⋯O、N-H⋯S、C-H⋯O和C-H⋯S氢键得以稳定。在晶体结构中还观察到Br⋯O相互作用[3.183 (3) Å]。
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