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2-(2,2,4-三甲基-6-对甲苯磺酰基-全氢-1,3-二氧杂环戊烯并[5,4-c]吡啶-5-基)乙酸甲酯

Methyl 2-(2,2,4-trimethyl-6-tosyl-perhydro-1,3-dioxino[5,4-c]pyridin-5-yl)acetate.

作者信息

Selvanayagam S, Sridhar B, Ravikumar K, Kathiravan S, Raghunathan R

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Apr 22;65(Pt 5):o1091. doi: 10.1107/S1600536809014391.

DOI:10.1107/S1600536809014391
PMID:21583906
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2977770/
Abstract

The title compound, C(20)H(29)NO(6)S, crystallizes with two mol-ecules in the asymmetric unit, with similar conformations. The dioxane and pyridine rings adopt twist conformations in both mol-ecules. The packing is stabilized by inter-molecular C-H⋯O hydrogen bonds.

摘要

标题化合物C(20)H(29)NO(6)S在不对称单元中以两个分子结晶，具有相似的构象。在两个分子中，二氧六环和吡啶环均呈扭曲构象。堆积通过分子间C-H⋯O氢键得以稳定。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b047/2977770/176e20b821d1/e-65-o1091-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b047/2977770/cdd3879dadbb/e-65-o1091-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b047/2977770/176e20b821d1/e-65-o1091-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b047/2977770/cdd3879dadbb/e-65-o1091-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b047/2977770/176e20b821d1/e-65-o1091-fig2.jpg

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本文引用的文献

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