Li Yu-Feng, Meng Fan-Yong
Acta Crystallogr Sect E Struct Rep Online. 2010 Sep 30;66(Pt 10):o2685. doi: 10.1107/S1600536810038389.
The title compound, C(12)H(17)N(3)S, was prepared by the reaction of 4-ethyl-thio-semicarbazide and 3,4-dimethyl-benzaldehyde. The dihedral angle between the thiourea unit and the benzene ring is 7.09 (8)°. In the crystal, inversion dimers linked by pairs of N-H⋯S hydrogen bonds occur.
标题化合物C(12)H(17)N(3)S由4-乙基硫代氨基脲与3,4-二甲基苯甲醛反应制备而成。硫脲单元与苯环之间的二面角为7.09 (8)°。在晶体中,通过N-H⋯S氢键对形成的反演二聚体存在。