5-[(4-乙氧羰基苯基)重氮基]苯-1,3-二羧酸二丁酯
Dibutyl 5-[(4-ethoxycarbonylphenyl)diazenyl]benzene-1,3-dicarboxylate.
作者信息
Liu Ying, Zhang Xianxi, Xue Zechun, Sheng Jian
机构信息
College of Chemistry and Chemical Engineering, Liaocheng University, Liaocheng, 252059, People's Republic of China.
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2010 Jun 23;66(Pt 7):o1730. doi: 10.1107/S1600536810022762.
Abstract
In the title compound, C(25)H(30)N(2)O(6), the dihedral angle between the aromatic rings is 3.79 (1) Å and the N=N bond shows a trans conformation. Both butyl side chains show evidence of disorder.
摘要
在标题化合物C₂₅H₃₀N₂O₆中，芳环之间的二面角为3.79 (1) Å，N=N键呈反式构象。两个丁基侧链均显示出无序的迹象。
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本文引用的文献
1
A short history of SHELX.
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
2
Design, synthesis, and photochemical behavior of poly(benzyl ester) dendrimers with azobenzene groups throughout their architecture.
J Org Chem. 2004 Dec 24;69(26):9073-84. doi: 10.1021/jo0499773.
3
About Dendrimers: Structure, Physical Properties, and Applications.
Chem Rev. 1999 Jul 14;99(7):1665-1688. doi: 10.1021/cr970069y.
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