4-氯-N-(4-硝基苯甲酰基)苯磺酰胺

4-Chloro-N-(4-nitro-benzo-yl)benzene-sulfonamide.

作者信息

Suchetan P A, Foro Sabine, Gowda B Thimme

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 Apr 1;67(Pt 4):o904. doi: 10.1107/S160053681100969X. Epub 2011 Mar 19.

DOI:10.1107/S160053681100969X

PMID:21754178

原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3099929/

Abstract

In the crystal structure of the title compound, C(13)H(9)ClN(2)O(5)S, the N-H bond is trans to the C=O bond (H-N-C-O torsion angle = 158.4°). The dihedral angle between the two aromatic rings is 87.8 (1)°. In the crystal, mol-ecules are linked into chains along the b axis via N-H⋯O hydrogen bonds.

摘要

在标题化合物C(13)H(9)ClN(2)O(5)S的晶体结构中，N-H键与C=O键呈反式（H-N-C-O扭转角 = 158.4°）。两个芳香环之间的二面角为87.8 (1)°。在晶体中，分子通过N-H⋯O氢键沿b轴连接成链。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/44da/3099929/cb3095dfccb2/e-67-0o904-fig1.jpg

相似文献

4-Chloro-N-(4-nitro-benzo-yl)benzene-sulfonamide.

Acta Crystallogr Sect E Struct Rep Online. 2011 Apr 1;67(Pt 4):o904. doi: 10.1107/S160053681100969X. Epub 2011 Mar 19.

2-Chloro-N-(4-nitro-benzo-yl)benzene-sulfonamide.

Acta Crystallogr Sect E Struct Rep Online. 2011 Apr 1;67(Pt 4):o930. doi: 10.1107/S1600536811009913. Epub 2011 Mar 19.

N-(3-Chloro-benzo-yl)-3-nitro-benzene-sulfonamide.

Acta Crystallogr Sect E Struct Rep Online. 2012 Jan;68(Pt 1):o244. doi: 10.1107/S1600536811054857. Epub 2011 Dec 23.

N-(2-Chloro-benzo-yl)-3-nitro-benzene-sulfonamide.

Acta Crystallogr Sect E Struct Rep Online. 2012 Feb 1;68(Pt 2):o543. doi: 10.1107/S1600536812003236. Epub 2012 Jan 31.

2-Methyl-N-(4-nitro-benzo-yl)benzene-sulfonamide.

Acta Crystallogr Sect E Struct Rep Online. 2011 Apr 1;67(Pt 4):o929. doi: 10.1107/S1600536811009846. Epub 2011 Mar 19.

N-(2-Chloro-phen-yl)-2-nitro-benzene-sulfonamide.

Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):o2575. doi: 10.1107/S1600536812033107. Epub 2012 Jul 28.

N-(3-Chloro-benzo-yl)-2-nitro-benzene-sulfonamide.

Acta Crystallogr Sect E Struct Rep Online. 2012 Mar 1;68(Pt 3):o786. doi: 10.1107/S160053681200640X. Epub 2012 Feb 17.

4-Chloro-N-(3-chloro-benzo-yl)benzene-sulfonamide monohydrate.

Acta Crystallogr Sect E Struct Rep Online. 2010 Jun 26;66(Pt 7):o1773. doi: 10.1107/S1600536810023962.

N-(3-Chloro-phen-yl)benzene-sulfonamide.

Acta Crystallogr Sect E Struct Rep Online. 2008 Aug 23;64(Pt 9):o1825. doi: 10.1107/S1600536808026895.

4-Chloro-N-(4-chloro-benzo-yl)benzene-sulfonamide.

Acta Crystallogr Sect E Struct Rep Online. 2010 May 8;66(Pt 6):o1253. doi: 10.1107/S160053681001559X.

引用本文的文献

Crystal structures of three N-(aryl-sulfon-yl)-4-fluoro-benzamides.

Acta Crystallogr E Crystallogr Commun. 2016 Mar 31;72(Pt 4):575-82. doi: 10.1107/S2056989016005089. eCollection 2016 Apr 1.

本文引用的文献

4-Methyl-N-(4-nitro-benzo-yl)benzene-sulfonamide.

Acta Crystallogr Sect E Struct Rep Online. 2011 Apr 1;67(Pt 4):o917. doi: 10.1107/S1600536811009470. Epub 2011 Mar 19.

4-Chloro-N-(4-chloro-benzo-yl)benzene-sulfonamide.

Acta Crystallogr Sect E Struct Rep Online. 2010 May 8;66(Pt 6):o1253. doi: 10.1107/S160053681001559X.

Structure validation in chemical crystallography.

Acta Crystallogr D Biol Crystallogr. 2009 Feb;65(Pt 2):148-55. doi: 10.1107/S090744490804362X. Epub 2009 Jan 20.

A short history of SHELX.

Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.

文献AI研究员

20分钟写一篇综述，助力文献阅读效率提升50倍。

立即体验

用中文搜PubMed

大模型驱动的PubMed中文搜索引擎

马上搜索

文档翻译

学术文献翻译模型，支持多种主流文档格式。

立即体验

4-氯-N-(4-硝基苯甲酰基)苯磺酰胺

4-Chloro-N-(4-nitro-benzo-yl)benzene-sulfonamide.

作者信息

出版信息

相似文献

引用本文的文献

本文引用的文献

文献AI研究员

用中文搜PubMed

文档翻译

Suppr 超能文献

4-氯-N-(4-硝基苯甲酰基)苯磺酰胺

4-Chloro-N-(4-nitro-benzo-yl)benzene-sulfonamide.

作者信息

出版信息