2-O-tert-Butyl-dimethyl-silyl-4,6-O-ethyl-idene-myo-insitol 1,3,5-orthoformate.
作者信息
Xu Zhouqin, Wang Qiang, Sun Yanchun
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2010 Jun 23;66(Pt 7):o1741. doi: 10.1107/S1600536810023214.
Abstract
In the title compound, C(15)H(26)O(6)Si, the dioxa six-membered ring bonded to the myo-inositol skeleton is in a boat conformation while the rest of the six-membered rings adopt chair conformations.
摘要
相似文献
1
2-O-tert-Butyl-dimethyl-silyl-4,6-O-ethyl-idene-myo-insitol 1,3,5-orthoformate.
Acta Crystallogr Sect E Struct Rep Online. 2010 Jun 23;66(Pt 7):o1741. doi: 10.1107/S1600536810023214.
2
Ethyl 1-O-tert-butyl-dimethyl-silyl-2,3-O-isopropyl-idene-5-[(2'S)-tetra-hydro-pyran-2-yl-oxy]-d-glycero-α-d-manno-hepto-furonate.
Acta Crystallogr Sect E Struct Rep Online. 2008 Jul 12;64(Pt 8):o1478. doi: 10.1107/S1600536808021193.
3
(1R,4S,8R,9R,12S,13S,14R,16S,17R,19R)-17-[(Ethyl-sulfan-yl)meth-yl]-9,14-di-hydroxy-7,7-dimethyl-2,18-dioxo-3,10-dioxapenta-cyclo[14.2.1.0.0.0]nona-decan-19-yl acetate acetone solvate.
Acta Crystallogr Sect E Struct Rep Online. 2008 Dec 24;65(Pt 1):o202. doi: 10.1107/S1600536808043341.
4
Neoline from Aconitum flavum Hand.
Acta Crystallogr Sect E Struct Rep Online. 2011 Jun 1;67(Pt 6):o1435. doi: 10.1107/S1600536811015170. Epub 2011 May 20.
5
8-O-Ethyl-yunaconitine from the roots of Aconitum carmichaeli Debx.
Acta Crystallogr Sect E Struct Rep Online. 2012 Jul 1;68(Pt 7):o2238. doi: 10.1107/S1600536812026463. Epub 2012 Jun 30.
6
Deltaline from Delphinium delavayi Franch.
Acta Crystallogr Sect E Struct Rep Online. 2011 Jan 22;67(Pt 2):o439. doi: 10.1107/S1600536811001681.
7
Bonvalotidine A acetone solvate from Delphinium bonvalotii Franch.
Acta Crystallogr Sect E Struct Rep Online. 2010 Nov 27;66(Pt 12):o3319. doi: 10.1107/S1600536810047562.
8
N-tert-Butyl-3-hydr-oxy-5-androstene-17-carboxamide monohydrate.
Acta Crystallogr Sect E Struct Rep Online. 2009 Jun 6;65(Pt 7):o1507-8. doi: 10.1107/S1600536809020984.
9
The first structural study on a cyclic tricoordinate phosphorochloridite and a pentacoordinate phosphorane based on 1,2,3,5-protected myo-inositol--a new conformation of 1,3,2-dioxaphosphorinane ring.
Carbohydr Res. 2007 Jul 2;342(9):1182-8. doi: 10.1016/j.carres.2007.02.031. Epub 2007 Mar 1.
10
Exciplex and excimer molecular probes: detection of conformational flip in a myo-inositol chair.
Org Biomol Chem. 2008 Jun 7;6(11):1966-72. doi: 10.1039/b800710a. Epub 2008 Apr 9.
本文引用的文献
1
A short history of SHELX.
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
2
Regioselective protection and deprotection of inositol hydroxyl groups.
Chem Rev. 2003 Nov;103(11):4477-503. doi: 10.1021/cr0200724.
3
myo-Inositol 4,6-carbonate: an easily prepared small molecule with three syn-axial hydroxyl groups.
Carbohydr Res. 2000 May 5;325(4):313-20. doi: 10.1016/s0008-6215(99)00306-7.
Zotero 插件