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1,3-双（4-甲氧基苄基）-6-甲基嘧啶-2,4（1H，3H）-二酮

1,3-Bis(4-meth-oxy-benz-yl)-6-methyl-pyrimidine-2,4(1H,3H)-dione.

作者信息

Li Gong-Chun, Zhang Li-Ke, Ju Zhi-Yu, Yang Feng-Ling

机构信息

College of Chemistry and Chemical Engineering, Xuchang University, Xuchang, Henan Province 461000, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 Jun 30;66(Pt 7):o1858. doi: 10.1107/S1600536810024815.

DOI:10.1107/S1600536810024815
PMID:21588055
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3006881/
Abstract

The title compound, C(21)H(22)N(2)O(4), was prepared by reaction of 6-methyl-pyrimidine-2,4(1H,3H)-dione and 1-chloro-methyl-4-meth-oxy-benzene. In the title mol-ecule, the central pyrimidine ring forms dihedral angles of 62.16 (4) and 69.77 (3)° with the two benzene rings. In the crystal, weak inter-molecular C-H⋯O hydrogen bonds link the mol-ecules into chains.

摘要

标题化合物C(21)H(22)N(2)O(4)是通过6-甲基嘧啶-2,4(1H,3H)-二酮与1-氯甲基-4-甲氧基苯反应制备的。在标题分子中，中心嘧啶环与两个苯环形成的二面角分别为62.16 (4)°和69.77 (3)°。在晶体中，弱的分子间C-H⋯O氢键将分子连接成链。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1c3d/3006881/67764b5afd93/e-66-o1858-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1c3d/3006881/184d795e722f/e-66-o1858-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1c3d/3006881/67764b5afd93/e-66-o1858-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1c3d/3006881/184d795e722f/e-66-o1858-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1c3d/3006881/67764b5afd93/e-66-o1858-fig2.jpg

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