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1,5 - 二甲基 - 3 - [(3 - 苯基 - 4,5 - 二氢 - 1,2 - 恶唑 - 5 - 基)甲基] - 1H - 1,5 - 苯并二氮杂䓬 - 2,4(3H,5H) - 二酮

1,5-Dimethyl-3-[(3-phenyl-4,5-dihydro-1,2-oxazol-5-yl)meth-yl]-1H-1,5-benzodiazepine-2,4(3H,5H)-dione.

作者信息

Dardouri Rachida, Kandri Rodi Youssef, Saffon Nathalie, El Ammari Lahcen, Essassi El Mokhtar

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 Oct 30;66(Pt 11):o2983. doi: 10.1107/S1600536810042972.

DOI:10.1107/S1600536810042972
PMID:21589149
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3009296/
Abstract

The reaction of 3-allyl-1,5-dimethyl-1,5-benzodiazepine-2,4-dione and benzaldoxime leads to the title compound, C(21)H(21)N(3)O(3). The mol-ecular structure is built up from two fused six- and seven-membered rings linked to a chain including a five- and six-membered ring (isoxazoline and phen-yl) via a methyl-ene group. The seven-membered ring displays a boat conformation. The dihedral angle between the two six-membered rings is 74.3 (1)°.

摘要

3-烯丙基-1,5-二甲基-1,5-苯并二氮杂䓬-2,4-二酮与苯甲醛肟反应生成标题化合物C(21)H(21)N(3)O(3)。分子结构由两个稠合的六元环和七元环组成，通过一个亚甲基与一个包含五元环和六元环（异恶唑啉和苯基）的链相连。七元环呈船式构象。两个六元环之间的二面角为74.3 (1)°。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d34d/3009296/0709e025ef3f/e-66-o2983-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d34d/3009296/0709e025ef3f/e-66-o2983-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d34d/3009296/0709e025ef3f/e-66-o2983-fig1.jpg

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