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（E，E）-3,3'-二甲基-1,1'-二苯基-4,4'-{[3-氮杂戊烷-1,5-二基双（氮杂二亚基）]双-（苯基亚甲基）}二-1H-吡唑-5（4H）-酮

(E,E)-3,3'-Dimethyl-1,1'-diphenyl-4,4'-{[3-aza-pentane-1,5-diylbis(aza-nedi-yl)]bis-(phenyl-methyl-idyne)}di-1H-pyrazol-5(4H)-one.

作者信息

Zhang Zhao-Po, Wang Yuan, Li Xiao-Xia, Li Yan-Wei

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 Nov 27;66(Pt 12):o3326. doi: 10.1107/S1600536810048981.

DOI:10.1107/S1600536810048981
PMID:21589602
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3011678/
Abstract

The asymmetric unit of the title compound, C(38)H(37)N(7)O(2), contains one half-mol-ecule, situated on a twofold rotational axis, in which one amino group is involved in intra-molecular N-H⋯O hydrogen bond and the two phenyl rings are twisted from the plane of pyrazolone ring by 26.69 (10) and 79.64 (8)°. The crystal packing exhibits no classical inter-molecular contacts.

摘要

标题化合物C(38)H(37)N(7)O(2)的不对称单元包含半个分子，位于一个二重旋转轴上，其中一个氨基参与分子内N-H⋯O氢键，两个苯环与吡唑啉酮环平面的扭转角度分别为26.69 (10)°和79.64 (8)°。晶体堆积中不存在典型的分子间相互作用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1416/3011678/245f19c8eb80/e-66-o3326-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1416/3011678/245f19c8eb80/e-66-o3326-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1416/3011678/245f19c8eb80/e-66-o3326-fig1.jpg

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