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5,5'-（丁烷-1,4-二基）双-（1H-四唑）二水合物

5,5'-(Butane-1,4-di-yl)bis-(1H-tetra-zole) dihydrate.

作者信息

Xin Jian-Hua, Tong Xiao-Lan

机构信息

College of Biology, Chemistry and Material Science, East China of Technology, 344000 Fuzhou, Jiangxi, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 Nov 27;66(Pt 12):o3328. doi: 10.1107/S1600536810048993.

DOI:10.1107/S1600536810048993
PMID:21589604
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3011479/
Abstract

The title compound, C(6)H(10)N(8)·2H(2)O, was prepared by the reaction of hexanedinitrile and sodium azide. The di-1H-tetra-zole mol-ecule lies on a crystallographic centre of inversion and is linked to the water mol-ecules by N-H⋯O and O-H⋯N hydrogen bonds, forming a two-dimensional supra-molecular structure in the crystal.

摘要

标题化合物C(6)H(10)N(8)·2H(2)O是通过己二腈与叠氮化钠反应制备的。二-1H-四唑分子位于一个晶体学反演中心上，并通过N-H⋯O和O-H⋯N氢键与水分子相连，在晶体中形成二维超分子结构。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f178/3011479/9ac393b1da4c/e-66-o3328-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f178/3011479/19b4fe3e08d0/e-66-o3328-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f178/3011479/9ac393b1da4c/e-66-o3328-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f178/3011479/19b4fe3e08d0/e-66-o3328-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f178/3011479/9ac393b1da4c/e-66-o3328-fig2.jpg

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本文引用的文献

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In situ hydrothermal synthesis of tetrazole coordination polymers with interesting physical properties.原位水热合成具有有趣物理性质的四唑配位聚合物。
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A short history of SHELX.SHELX简史。
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A pcu-type metal-organic framework with spindle [Zn7(OH)8]6+ cluster as secondary building units.
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