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N-（4-甲基苯基）-N'-苯基丁二酰胺一水合物

N-(4-Methyl-phen-yl)-N'-phenyl-butane-diamide monohydrate.

作者信息

Saraswathi B S, Foro Sabine, Gowda B Thimme

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 Jun 1;67(Pt 6):o1495. doi: 10.1107/S1600536811018915. Epub 2011 May 25.

DOI:10.1107/S1600536811018915
PMID:21754863
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3120322/
Abstract

In the title hydrate, C(17)H(18)N(2)O(2)·H(2)O, the dihedral angles formed by the aromatic rings of the benzene and methyl-benzene groups with the mean planes of the attached NH-C(O)-CH(2) fragments are 12.6 (4) and 23.3 (3)°, respectively, while that between the two aromatic rings is 73.7 (2)°. In the crystal, the water mol-ecule accepts two and makes two hydrogen bonds. The mol-ecules are packed into layers parallel to (101) by O-H⋯O and N-H⋯O hydrogen-bonding inter-actions.

摘要

在标题水合物C(17)H(18)N(2)O(2)·H(2)O中，苯环和甲基苯环的芳香环与相连的NH-C(O)-CH(2)片段平均平面形成的二面角分别为12.6 (4)°和23.3 (3)°，而两个芳香环之间的二面角为73.7 (2)°。在晶体中，水分子接受两个并形成两个氢键。分子通过O-H⋯O和N-H⋯O氢键相互作用堆积成平行于(101)的层。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0143/3120322/e0c2be7c3ddd/e-67-o1495-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0143/3120322/2520eb0dc7ab/e-67-o1495-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0143/3120322/e0c2be7c3ddd/e-67-o1495-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0143/3120322/2520eb0dc7ab/e-67-o1495-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0143/3120322/e0c2be7c3ddd/e-67-o1495-fig2.jpg

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