Saraswathi B S, Foro Sabine, Gowda B Thimme
Acta Crystallogr Sect E Struct Rep Online. 2011 Jun 1;67(Pt 6):o1495. doi: 10.1107/S1600536811018915. Epub 2011 May 25.
In the title hydrate, C(17)H(18)N(2)O(2)·H(2)O, the dihedral angles formed by the aromatic rings of the benzene and methyl-benzene groups with the mean planes of the attached NH-C(O)-CH(2) fragments are 12.6 (4) and 23.3 (3)°, respectively, while that between the two aromatic rings is 73.7 (2)°. In the crystal, the water mol-ecule accepts two and makes two hydrogen bonds. The mol-ecules are packed into layers parallel to (101) by O-H⋯O and N-H⋯O hydrogen-bonding inter-actions.
在标题水合物C(17)H(18)N(2)O(2)·H(2)O中,苯环和甲基苯环的芳香环与相连的NH-C(O)-CH(2)片段平均平面形成的二面角分别为12.6 (4)°和23.3 (3)°,而两个芳香环之间的二面角为73.7 (2)°。在晶体中,水分子接受两个并形成两个氢键。分子通过O-H⋯O和N-H⋯O氢键相互作用堆积成平行于(101)的层。