Division of Orthodontics and Dentofacial Orthopedics, Department of Oral Growth and Development, School of Dentistry, Health Sciences University of Hokkaido, Ishikari-Tobetsu, Japan.
Eur J Orthod. 2013 Apr;35(2):216-22. doi: 10.1093/ejo/cjr113. Epub 2011 Sep 20.
This study investigated the effects of a diamond-like carbon (DLC) coating on frictional and mechanical properties of orthodontic brackets. DLC films were deposited on stainless steel brackets using the plasma-based ion implantation/deposition (PBIID) method under two different atmospheric conditions. As-received metal brackets served as the control. Two sizes of stainless steel archwires, 0.018 inch diameter and 0.017 × 0.025 inch cross-section dimensions, were used for measuring static and kinetic friction by drawing the archwires through the bracket slots, using a mechanical testing machine (n = 10). The DLC-coated brackets were observed with a scanning electron microscope (SEM). Values of hardness and elastic modulus were obtained by nanoindentation testing (n = 10). Friction forces were compared by one-way analysis of variance and the Scheffé test. The hardness and elastic modulus of the brackets were compared using Kruskal-Wallis and Mann-Whitney U-tests. SEM photomicrographs showed DLC layers on the bracket surfaces with thickness of approximately 5-7 μm. DLC-coated brackets deposited under condition 2 showed significantly less static frictional force for the stainless steel wire with 0.017 × 0.025 inch cross-section dimensions than as-received brackets and DLC-coated brackets deposited under condition 1, although both DLC-coated brackets showed significantly less kinetic frictional force than as-received brackets. The hardness of the DLC layers was much higher than that of the as-received bracket surfaces. In conclusion, the surfaces of metal brackets can be successfully modified by the PBIID method to create a DLC layer, and the DLC-coating process significantly reduces frictional forces.
本研究探讨了类金刚石碳(DLC)涂层对正畸托槽摩擦和机械性能的影响。采用等离子体基离子注入/沉积(PBIID)方法,在两种不同的大气条件下在不锈钢托槽上沉积 DLC 薄膜。原始金属托槽作为对照。使用两种尺寸的不锈钢弓丝,直径为 0.018 英寸和 0.017×0.025 英寸横截面尺寸,通过机械试验机(n=10)在托槽槽中拉动弓丝来测量静摩擦和动摩擦。使用扫描电子显微镜(SEM)观察 DLC 涂层托槽。通过纳米压痕试验(n=10)获得硬度和弹性模量值。通过单向方差分析和 Scheffé 检验比较摩擦力。使用 Kruskal-Wallis 和 Mann-Whitney U 检验比较托槽的硬度和弹性模量。SEM 显微照片显示托槽表面有厚度约为 5-7μm 的 DLC 层。与原始托槽和在条件 1 下沉积的 DLC 涂层托槽相比,在条件 2 下沉积的 DLC 涂层托槽对横截面尺寸为 0.017×0.025 英寸的不锈钢丝显示出显著较小的静摩擦力,尽管两种 DLC 涂层托槽显示出的动摩擦力均显著小于原始托槽。DLC 层的硬度远高于原始托槽表面的硬度。总之,PBIID 方法可以成功地对金属托槽表面进行改性,以形成 DLC 层,并且 DLC 涂层过程显著降低了摩擦力。