一种简便易行的合成方法，用于合成一些含有噻吩并[2,3-b]噻吩的新型腙、席夫碱和吡唑。
A facile and convenient synthesis of some novel hydrazones, Schiff's base and pyrazoles incorporating thieno[2,3-b]thiophenes.
作者信息
Mabkhot Yahia Nasser, Barakat Assem, Al-Majid Abdullah Mohammed, Al-Othman Zeid Abdullah, Alamary Abdullah Saleh
机构信息
Department of Chemistry, Faculty of Science, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia; E-Mails:
出版信息
Int J Mol Sci. 2011;12(11):7824-34. doi: 10.3390/ijms12117824. Epub 2011 Nov 11.
A facile and convenient synthesis of some novel hydrazones, schiff's base and pyrazoles from thieno[2,3-b]thiophene derivatives 1 have been achieved in high yields assisted by microwave and classical methods. The structures of all the title compounds have been elucidated by elemental analysis, IR, MS, (1)H-NMR and (13)C-NMR. Generally, these findings represent a new class of sulfur and nitrogen moieties that should also be of interest as new materials.
在微波和传统方法的辅助下，已经以高产率实现了从噻吩并[2,3 - b]噻吩衍生物1简便方便地合成一些新型腙、席夫碱和吡唑。所有标题化合物的结构均通过元素分析、红外光谱、质谱、¹H - NMR和¹³C - NMR进行了阐明。一般来说，这些发现代表了一类新的硫和氮部分，作为新材料也应该会引起人们的兴趣。
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