Felizardo Klíssia Romero, Lemos Letícia Vargas Freire Martins, de Carvalho Rodrigo Varella, Gonini Junior Alcides, Lopes Murilo Baena, Moura Sandra Kiss
Dental School, University North of Paraná, Londrina, PR, Brazil.
Braz Dent J. 2011;22(6):468-72. doi: 10.1590/s0103-64402011000600005.
This study analyzed the bond strength (BS) of HEMA versus HEMA-free self-etch adhesive systems to dentin. The occlusal surface of 20 third molars was removed and the dentin was abraded with 600-grit silicon carbide paper. The teeth were randomly assigned to 4 groups (n = 5) and restored with GO, Adper SE Plus, OptiBond All-In-One, and Clearfil 3S Bond adhesive systems and Filtek Z350 composite. After light curing (600 mW/cm²), the teeth were stored in distilled water at 37 ºC for 24 h and were sectioned in the mesiodistal and buccolingual directions to obtain sticks (0.8 mm²). The sticks were subjected to tensile force using a universal testing machine (0.5 mm/min), and the modes of failure were analyzed by scanning electron microscopy and classified as adhesive, cohesive, or mixed. The BS data (in MPa) were treated using one-way ANOVA and Tukey's tests at 5% significance. GO presented the lowest mean bond strength value (10.57 ± 3.72) and differed significantly from the other materials (p = 0.001), which, in turn, presented statistically similar results (p>0.05) among themselves: Adper SE Plus (29.08 ± 8.93), OptiBond All-In-One (28.36 ± 6.49), and Clearfil 3S Bond (28.62 ± 6.97). Mixed fractures were the most prevalent. It was concluded that the influence of HEMA on BS to dentin was material dependent.
本研究分析了含甲基丙烯酸羟乙酯(HEMA)与不含HEMA的自酸蚀粘结系统与牙本质之间的粘结强度(BS)。去除20颗第三磨牙的咬合面,并用600目碳化硅砂纸打磨牙本质。将牙齿随机分为4组(n = 5),分别用GO、Adper SE Plus、OptiBond All-In-One和Clearfil 3S Bond粘结系统及Filtek Z350复合树脂进行修复。光固化(600 mW/cm²)后,将牙齿在37 ºC的蒸馏水中储存24小时,然后沿近远中方向和颊舌方向切片以获得小棒(0.8 mm²)。使用万能试验机(0.5 mm/min)对小棒施加拉力,并通过扫描电子显微镜分析断裂模式,分为粘结性、内聚性或混合性。BS数据(以MPa为单位)采用单因素方差分析和Tukey检验进行处理,显著性水平为5%。GO的平均粘结强度值最低(10.57 ± 3.72),与其他材料有显著差异(p = 0.001),而其他材料之间的结果在统计学上相似(p>0.05):Adper SE Plus(29.08 ± 8.93)、OptiBond All-In-One(28.36 ± 6.49)和Clearfil 3S Bond(28.62 ± 6.97)。混合性断裂最为常见。研究得出结论,HEMA对与牙本质粘结强度的影响取决于材料。