Wu Xuefen, Chen Xi, Hou Yimin
Acta Crystallogr Sect E Struct Rep Online. 2011 Dec 1;67(Pt 12):o3482. doi: 10.1107/S1600536811049749. Epub 2011 Nov 30.
The title compound, C(18)H(28)N(4)O(6), crystallizes with two mol-ecules in the asymmetric unit which differ slightly in conformation. The dihedral angle between the amide plane and the benzene ring are 72.6 (2) and 66.8 (2)° in the two mol-ecules. A strong intra-molecular N-H⋯O hydrogen bond between the amino and nitro groups occurs in each mol-ecule. The crystal structure features two symmetry-independent polymeric chains along [010] generated by N-H⋯O hydrogen bonds between the amide groups.
标题化合物C(18)H(28)N(4)O(6)在不对称单元中结晶,含有两个构象略有不同的分子。两个分子中酰胺平面与苯环之间的二面角分别为72.6 (2)°和66.8 (2)°。每个分子中氨基和硝基之间存在强的分子内N-H⋯O氢键。晶体结构的特征是沿着[010]方向有两条由酰胺基团之间的N-H⋯O氢键产生的独立对称聚合链。