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（E）-1-[2-羟基-4,6-双（甲氧基甲氧基）苯基]-3-[3-甲氧基-4-（甲氧基甲氧基）苯基]丙-2-烯-1-酮

(E)-1-[2-Hy-droxy-4,6-bis-(meth-oxy-meth-oxy)phen-yl]-3-[3-meth-oxy-4-(meth-oxy-meth-oxy)phen-yl]prop-2-en-1-one.

作者信息

Chang Liu-Shuan, Li Chen-Yang, Zhao Yan-Mei, Xu Fang, Gu Zheng-Yi

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 Nov;67(Pt 11):o2931. doi: 10.1107/S1600536811041213. Epub 2011 Oct 12.

DOI:10.1107/S1600536811041213
PMID:22219962
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3247344/
Abstract

The title compound, C(22)H(26)O(9), crystallizes with two independent mol-ecules in the asymmetric unit in which the dihedral angles between the two benzene rings are 21.4 (2) and 5.1 (2)°. An intra-molecular O-H⋯O hydrogen bond occurs in each mol-ecule. Inter-molecular C-H⋯O hydrogen bonds stabilize the crystal structure.

摘要

标题化合物C(22)H(26)O(9)在不对称单元中以两个独立分子结晶，其中两个苯环之间的二面角分别为21.4 (2)°和5.1 (2)°。每个分子中均存在分子内O-H⋯O氢键。分子间C-H⋯O氢键使晶体结构得以稳定。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3ecd/3247344/71ed37ebcf16/e-67-o2931-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3ecd/3247344/71ed37ebcf16/e-67-o2931-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3ecd/3247344/71ed37ebcf16/e-67-o2931-fig1.jpg

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