• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利：CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法，用中文像聊天一样搜索，搜遍4000万医学文献。AI智能推荐，让科研检索更轻松。

立即免费搜索

文件翻译

保留排版，准确专业，支持PDF/Word/PPT等文件格式，支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述，25分钟生成高质量综述，智能提取关键信息，辅助科研写作。

立即免费体验

2-氨基-4-(2-氯苯基)-5-氧代-5,6,7,8-四氢-4H-色烯-3-甲腈乙醇单溶剂合物

2-Amino-4-(2-chloro-phen-yl)-5-oxo-5,6,7,8-tetra-hydro-4H-chromene-3-carbonitrile ethanol monosolvate.

作者信息

Qiao Yan, Kong Lingqian, Chen Guifang, Li Shengli, Gao Zhiqing

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 Nov;67(Pt 11):o3099. doi: 10.1107/S1600536811043650. Epub 2011 Oct 29.

DOI:10.1107/S1600536811043650
PMID:22220103
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3247485/
Abstract

In the title compound, C(16)H(13)ClN(2)O(2)·C(2)H(6)O, the fused cyclo-hexene and pyran rings adopt envelope and flattened boat conformations, respectively. In the crystal, N-H⋯O and O-H⋯O hydrogen bonds link the chromene and ethanol solvent mol-ecules into infinite chains along the c axis, and N-H⋯N hydrogen bonds link these chains into a three-dimensional framework. Weak C-H⋯π inter-actions are also present.

摘要

在标题化合物C(16)H(13)ClN(2)O(2)·C(2)H(6)O中，稠合的环己烯环和吡喃环分别呈信封式和扁平船式构象。在晶体中，N-H⋯O和O-H⋯O氢键将色烯和乙醇溶剂分子沿c轴连接成无限链，且N-H⋯N氢键将这些链连接成三维框架。还存在弱的C-H⋯π相互作用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f6e3/3247485/906c2f71ac7f/e-67-o3099-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f6e3/3247485/5cb30e2d31ad/e-67-o3099-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f6e3/3247485/906c2f71ac7f/e-67-o3099-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f6e3/3247485/5cb30e2d31ad/e-67-o3099-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f6e3/3247485/906c2f71ac7f/e-67-o3099-fig2.jpg

相似文献

1
2-Amino-4-(2-chloro-phen-yl)-5-oxo-5,6,7,8-tetra-hydro-4H-chromene-3-carbonitrile ethanol monosolvate.2-氨基-4-(2-氯苯基)-5-氧代-5,6,7,8-四氢-4H-色烯-3-甲腈乙醇单溶剂合物
Acta Crystallogr Sect E Struct Rep Online. 2011 Nov;67(Pt 11):o3099. doi: 10.1107/S1600536811043650. Epub 2011 Oct 29.
2
2-Amino-4-(4-chloro-phen-yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra-hydro-4H-chromene-3-carbonitrile propan-2-one monosolvate.2-氨基-4-（4-氯苯基）-7,7-二甲基-5-氧代-5,6,7,8-四氢-4H-色烯-3-腈丙-2-酮单溶剂合物
Acta Crystallogr Sect E Struct Rep Online. 2012 Jun 1;68(Pt 6):o1965-6. doi: 10.1107/S1600536812024142. Epub 2012 May 31.
3
2-Amino-4-(4-chloro-phen-yl)-5-oxo-5,6,7,8-tetra-hydro-4H-chromene-3-carbonitrile.2-氨基-4-（4-氯苯基）-5-氧代-5,6,7,8-四氢-4H-色烯-3-腈
Acta Crystallogr Sect E Struct Rep Online. 2012 May 1;68(Pt 5):o1414-5. doi: 10.1107/S1600536812015838. Epub 2012 Apr 18.
4
2-Amino-5-oxo-4-phenyl-5,6,7,8-tetra-hydro-4H-chromene-3-carbonitrile.2-氨基-5-氧代-4-苯基-5,6,7,8-四氢-4H-色烯-3-腈
Acta Crystallogr Sect E Struct Rep Online. 2011 Apr 1;67(Pt 4):o832. doi: 10.1107/S1600536811008130. Epub 2011 Mar 9.
5
2-Amino-4-(2-chloro-phen-yl)-7,7-di-methyl-5-oxo-5,6,7,8-tetra-hydro-4H-chromene-3-carbonitrile hemihydrate.2-氨基-4-(2-氯苯基)-7,7-二甲基-5-氧代-5,6,7,8-四氢-4H-色烯-3-腈半水合物
Acta Crystallogr Sect E Struct Rep Online. 2012 Mar 1;68(Pt 3):o823. doi: 10.1107/S1600536812003807. Epub 2012 Feb 24.
6
2-Amino-7,7-dimethyl-5-oxo-4-[3-(trifluoro-meth-yl)phen-yl]-5,6,7,8-tetra-hydro-4H-chromene-3-carbonitrile.2-氨基-7,7-二甲基-5-氧代-4-[3-(三氟甲基)苯基]-5,6,7,8-四氢-4H-色烯-3-腈
Acta Crystallogr Sect E Struct Rep Online. 2013 Mar 1;69(Pt 3):o417-8. doi: 10.1107/S1600536813004522. Epub 2013 Feb 20.
7
2-Amino-4-(4-methyl-phen-yl)-5-oxo-5,6,7,8-tetra-hydro-4H-chromene-3-carbonitrile.2-氨基-4-（4-甲基苯基）-5-氧代-5,6,7,8-四氢-4H-色烯-3-腈
Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):o2315-6. doi: 10.1107/S1600536812029480. Epub 2012 Jul 4.
8
2-Amino-4-(4-meth-oxy-phen-yl)-7,7-di-methyl-5-oxo-5,6,7,8-tetra-hydro-4H-chromene-3-carbonitrile propan-2-one monosolvate.2-氨基-4-（4-甲氧基苯基）-7,7-二甲基-5-氧代-5,6,7,8-四氢-4H-色烯-3-腈丙-2-酮单溶剂合物
Acta Crystallogr Sect E Struct Rep Online. 2012 Jul 1;68(Pt 7):o2206-7. doi: 10.1107/S160053681202781X. Epub 2012 Jun 27.
9
2-Amino-4-[4-(dimethyl-amino)-phen-yl]-5-oxo-5,6,7,8-tetra-hydro-4H-chromene-3-carbonitrile.2-氨基-4-[4-(二甲基氨基)-苯基]-5-氧代-5,6,7,8-四氢-4H-色烯-3-腈
Acta Crystallogr Sect E Struct Rep Online. 2011 Nov;67(Pt 11):o3067. doi: 10.1107/S1600536811043662. Epub 2011 Oct 29.
10
2-Amino-7,7-dimethyl-5-oxo-4-(p-tol-yl)-5,6,7,8-tetra-hydro-4H-chromene-3-carbonitrile.2-氨基-7,7-二甲基-5-氧代-4-（对甲苯基）-5,6,7,8-四氢-4H-色烯-3-甲腈
Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):o2592-3. doi: 10.1107/S1600536812033570. Epub 2012 Jul 28.

引用本文的文献

1
2-Amino-4-(4-chloro-phen-yl)-5-oxo-5,6,7,8-tetra-hydro-4H-chromene-3-carbonitrile.2-氨基-4-（4-氯苯基）-5-氧代-5,6,7,8-四氢-4H-色烯-3-腈
Acta Crystallogr Sect E Struct Rep Online. 2012 May 1;68(Pt 5):o1414-5. doi: 10.1107/S1600536812015838. Epub 2012 Apr 18.

本文引用的文献

1
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.