Hua D H, Bharathi S N, Tsujimoto A, Robinson P D
Department of Chemistry, Kansas State University, Manhattan 66506.
Acta Crystallogr C. 1990 Jul 15;46 ( Pt 7):1306-8. doi: 10.1107/s0108270189011601.
C16H19NO2S, Mr = 289.39, orthorhombic, P2(1)2(1)2(1), a = 11.467 (5), b = 17.207 (8), c = 7.566 (4) A, V = 1493 (2) A3, Z = 4, Dx = 1.29 g cm-3, lambda(Mo K alpha) = 0.71069 A, mu = 2.07 cm-1, F(000) = 616, T = 296 K, R = 0.049, 928 unique observed reflections. The structure determination combined with the known S configuration at the sulfur site discloses the stereochemistry of the title compound to be 7S and SS.
C₁₆H₁₉NO₂S，Mr = 289.39，正交晶系，P2(1)2(1)2(1)，a = 11.467(5)，b = 17.207(8)，c = 7.566(4)埃，V = 1493(2)埃³，Z = 4，Dx = 1.29克/厘米³，λ(Mo Kα) = 0.71069埃，μ = 2.07厘米⁻¹，F(000) = 616，T = 296K，R = 0.049，928个独立观测反射。结构测定结合硫位点已知的S构型揭示标题化合物的立体化学为7S和SS。
