National Metal and Materials Technology Center (MTEC), 114 Thailand Science Park, Pathumthani 12120, Thailand.
Dent Mater J. 2012 Feb 3;31(1):125-30. doi: 10.4012/dmj.2011-136. Epub 2012 Jan 21.
In this paper, we report on the enhanced strength of glass ionomer cement (GIC) by using the process of pre acid-base reaction and spray drying in glass preparation. The pre acid-base reaction was induced by prior mixing of the glass powder with poly(alkenoic acid). The weight ratios of glass powder to poly(alkenoic acid) were varied to investigate the extent of the pre acid-base reaction of the glass. The effect of the spray drying process which produced spherical glass particles on cement strength was also studied and discussed. The results show that adding 2%-wt of poly(alkenoic acid) liquid in the pre-reacted step improved cement strength. GICs prepared using a mixture of pre-reacted glass with both spherical and irregular powders at 60:40 by weight exhibited the highest compressive strength at 138.64±7.73 MPa. It was concluded that glass ionomer cements containing pre-reacted glass with mixed glass morphology using both spherical and irregular forms are promising as restorative dental materials with improved mechanical properties and handling characteristics.
本文报告了通过在玻璃制备过程中采用预酸碱反应和喷雾干燥的方法来提高玻璃离子体水泥(GIC)的强度。预酸碱反应是通过将玻璃粉末与聚烯酸预先混合来引发的。改变玻璃粉末与聚烯酸的重量比来研究玻璃的预酸碱反应程度。还研究和讨论了喷雾干燥过程对水泥强度的影响,该过程产生了球形玻璃颗粒。结果表明,在预反应步骤中添加 2%wt 的聚烯酸液体可以提高水泥强度。使用预反应玻璃与 60:40 重量比的球形和不规则粉末的混合物制备的 GIC 表现出最高的抗压强度,为 138.64±7.73 MPa。结论是,含有预反应玻璃的玻璃离子体水泥,混合了球形和不规则形状的玻璃形态,有望成为具有改善的机械性能和处理特性的修复牙科材料。