Kroner E, Blau J, Arzt E
INM-Leibniz Institute for New Materials, Saarbrucken, Germany.
Rev Sci Instrum. 2012 Jan;83(1):016101. doi: 10.1063/1.3675888.
Current adhesion measurement setups designed for experiments on bioinspired fibrillar surfaces, either commercial or constructed in-house, do not allow adhesion measurements with in situ visualization, high resolution, high force range, and controlled alignment at the same time. In this paper a new adhesion tester is presented, which enables contact experiments with controlled tilt angle (accuracy of ±0.02°). This allows the use of flat probes and thus greatly simplifies the determination of experimental parameters such as pull-off strength or Young's modulus. The deflection of a double-clamped glass beam is measured by laser interferometry with an accuracy of ±60 nm, which yields a precise force measurement over three orders of magnitude force range without changing the glass beam. Contact formation and detachment events can be visualized in situ. The current adhesion tester is designed for force measurements in the range of 1 μN to 1 N and fills the gap between macroscopic tests and atomic force microscopy measurements.
目前用于生物启发纤维表面实验的粘附力测量装置,无论是商用的还是内部构建的,都无法同时进行原位可视化、高分辨率、高力范围和可控对准的粘附力测量。本文提出了一种新型粘附力测试仪,它能够进行具有可控倾斜角度(精度为±0.02°)的接触实验。这允许使用扁平探针,从而极大地简化了诸如剥离强度或杨氏模量等实验参数的测定。通过激光干涉测量法测量双夹玻璃梁的挠度,精度为±60 nm,无需更换玻璃梁即可在三个数量级的力范围内进行精确的力测量。接触形成和分离事件可以原位可视化。当前的粘附力测试仪设计用于1 μN至1 N范围内的力测量,填补了宏观测试和原子力显微镜测量之间的空白。