（2E，6E）-2,6-双（2,6-二氯苄叉基）环己酮
(2E,6E)-2,6-Bis(2,6-dichloro-benzyl-idene)-cyclo-hexa-none.
作者信息
Mahdavinia Gholam Hossein, Mirzazadeh Maryam, Amani Vahid, Notash Behrouz
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2012 Mar 1;68(Pt 3):o778. doi: 10.1107/S1600536812006629. Epub 2012 Feb 17.
Abstract
The title compound, C(20)H(14)Cl(4)O, was prepared by the reaction of 2,6-dichloro-benzaldehyde and cyclo-hexa-none. In the mol-ecule, the central cyclo-hexa-none ring adopts an envelope conformation, while the terminal benzene rings make a dihedral angle of 57.87 (9)°.
摘要
标题化合物C(20)H(14)Cl(4)O是通过2,6-二氯苯甲醛与环己酮反应制备的。在分子中，中心环己酮环呈信封构象，而末端苯环形成的二面角为57.87 (9)°。
相似文献
1
(2E,6E)-2,6-Bis(2,6-dichloro-benzyl-idene)-cyclo-hexa-none.（2E，6E）-2,6-双（2,6-二氯苄叉基）环己酮
Acta Crystallogr Sect E Struct Rep Online. 2012 Mar 1;68(Pt 3):o778. doi: 10.1107/S1600536812006629. Epub 2012 Feb 17.
2
(2E,6E)-2,6-Bis(4-ethoxy-benzyl-idene)cyclo-hexa-none.（2E，6E）-2,6-双（4-乙氧基-亚苄基）环己酮
Acta Crystallogr Sect E Struct Rep Online. 2008 Oct 25;64(Pt 11):o2199. doi: 10.1107/S1600536808034272.
3
(2E,5E)-2,5-Bis(3,4,5-trimethoxy-benzyl-idene)cyclo-penta-none.(2E,5E)-2,5-双(3,4,5-三甲氧基-亚苄基)环戊酮
Acta Crystallogr Sect E Struct Rep Online. 2008 Sep 20;64(Pt 10):o1964. doi: 10.1107/S1600536808029474.
4
(2E,6E)-2,6-Bis(ferrocenyl-methyl-idene)cyclo-hexa-none dichloro-methane monosolvate.（2E，6E）-2,6-双（二茂铁基亚甲基）环己酮二氯甲烷单溶剂合物
Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):m1064. doi: 10.1107/S1600536812030899. Epub 2012 Jul 14.
5
(2E,6E)-2,6-Bis(2,4,5-trimethoxy-benzyl-idene)cyclo-hexa-none.
Acta Crystallogr Sect E Struct Rep Online. 2010 Feb 13;66(Pt 3):o630-1. doi: 10.1107/S1600536810005192.
6
2,6-Bis(4-methoxy-benzyl-idene)cyclo-hexa-none.2,6-双（4-甲氧基-亚苄基）环己酮
Acta Crystallogr Sect E Struct Rep Online. 2009 Mar 31;65(Pt 4):o928. doi: 10.1107/S160053680901112X.
7
2,6-Bis(2,4-dichloro-benzyl-idene)cyclo-hexa-none.2,6-双（2,4-二氯亚苄基）环己酮
Acta Crystallogr Sect E Struct Rep Online. 2008 Jul 31;64(Pt 8):o1626. doi: 10.1107/S1600536808023003.
8
2,6-Bis(2-chloro-benzyl-idene)cyclo-hexanone.2,6-双（2-氯亚苄基）环己酮
Acta Crystallogr Sect E Struct Rep Online. 2009 Mar 6;65(Pt 4):o694. doi: 10.1107/S1600536809007648.
9
(2E,6E)-2,6-Bis(2,5-difluoro-benzyl-idene)cyclo-hexa-none.（2E，6E）-2,6-双（2,5-二氟亚苄基）环己酮
Acta Crystallogr Sect E Struct Rep Online. 2010 Apr 2;66(Pt 5):o1009. doi: 10.1107/S1600536810011499.
10
(2E,6E)-2,6-Bis(4-methyl-benzyl-idene)cyclo-hex-3-en-1-one.（2E，6E）-2,6-双（4-甲基-亚苄基）环己-3-烯-1-酮
Acta Crystallogr Sect E Struct Rep Online. 2012 Feb 1;68(Pt 2):o355. doi: 10.1107/S1600536811055632. Epub 2012 Jan 11.
引用本文的文献
1
Synthesis, characterization, quantum mechanical calculations and biomedical docking studies on curcumin analogs: 2, 6-(Difurfurylidene) cyclohexanone and 2, 6 - Bis (2,6-Dichloro Benzylidene) Cyclohexanone.姜黄素类似物：2,6 -（二糠叉基）环己酮和2,6 - 双（2,6 - 二氯亚苄基）环己酮的合成、表征、量子力学计算及生物医学对接研究
Heliyon. 2024 Sep 27;10(19):e38300. doi: 10.1016/j.heliyon.2024.e38300. eCollection 2024 Oct 15.
本文引用的文献
1
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
2
Cytotoxic analogues of 2,6-bis(arylidene)cyclohexanones.2,6-双（亚芳基）环己酮的细胞毒性类似物
Eur J Med Chem. 2003 Feb;38(2):169-77. doi: 10.1016/s0223-5234(02)01444-7.
3
Synthesis, antimicrobial and antifungal activity of a new class of spiro pyrrolidines.一类新型螺环吡咯烷的合成、抗菌和抗真菌活性
Bioorg Med Chem. 2003 Feb 6;11(3):407-19. doi: 10.1016/s0968-0896(02)00439-x.
4
Strategies for structure solution and refinement of small organic molecules from electron diffraction data and limitations of the simulation approach.基于电子衍射数据的小分子结构解析与精修策略及模拟方法的局限性
Acta Crystallogr A. 2000 Sep;56 (Pt 5):436-50. doi: 10.1107/s0108767300006668.
5
[Potentially bioactive pyrimidine derivatives. 1. 2-Amino-4-aryl-8-arylidene-3,4,5,6,7,8-hexahydroquinazoline].
Pharmazie. 1984 Aug;39(8):539-40.
Zotero 插件