Silva Emerson H, Albuquerque Rodrigo C, Lanza Lincoln D, Vieira Guilherme C, Peixoto Rogéli T R C, Alvim Hugo H, Yoshida Maria I
Department of Restorative Dentistry, School of Dentistry, Federal University of Minas Gerais, Belo Horizonte, Brazil.
Indian J Dent Res. 2011 Nov-Dec;22(6):790-4. doi: 10.4103/0970-9290.94670.
The purpose of this paper was to evaluate the influence of different light curing units on the conversion of four composite resins with different compositions (Durafill VS - Heraeus-Kulzer, Tetric Ceram - Ivoclar/Vivadent, Filtek Supreme XT - 3M ESPE e Aelite LS Packable - Bisco), using differential scanning calorimetry.
A stainless steel matrix was used to prepare 48 cylindrical composite test samples (n=6), measuring 3 mm in diameter and 1 mm in thickness. The samples were photoactivated using a halogen lamp (Optilux 500 - Demetron/Kerr) and three different generations of light-emitting diodes (LEDs) (LEC-470 I - MMOptics, Radii Plus - SDI and Ultra-Lume LED 5 - Ultradent). After removal of the matrix, each sample was weighed and hermetically sealed in an aluminum pan and analyzed. The amount of heat liberated by thermopolymerisation of residual monomers after photoactivation was measured in Joules/gram (J/g). The data were submitted to Analysis of Variance (ANOVA) test (P ≤ 0.002) and the Tukey test (P < 0.05).
The Ultra-Lume LED 5 was superior on degree of conversion for all resins. The Radii Plus was equal to the Ultra-Lume LED 5, except for the resin Tetric Ceram , were the Optilux 500 was superior. The LEC-470 I was inferior for the conversion of all resins.
The study proves the importance of the compatibility of the different photoinitiators in resin composites with the different light sources.
本文旨在使用差示扫描量热法评估不同光固化设备对四种不同成分复合树脂(Durafill VS - 贺利氏古莎公司、Tetric Ceram - 义获嘉伟瓦登特公司、Filtek Supreme XT - 3M 公司和Aelite LS Packable - Bisco公司)转化率的影响。
使用不锈钢模具制备48个圆柱形复合树脂测试样品(n = 6),直径3毫米,厚度1毫米。使用卤素灯(Optilux 500 - Demetron/Kerr)和三代不同的发光二极管(LED)(LEC - 470 I - MMOptics公司、Radii Plus - SDI公司和Ultra - Lume LED 5 - Ultradent公司)对样品进行光固化。去除模具后,对每个样品称重并密封在铝盘中进行分析。测量光固化后残留单体热聚合释放的热量,单位为焦耳/克(J/g)。数据进行方差分析(ANOVA检验,P≤0.002)和Tukey检验(P < 0.05)。
Ultra - Lume LED 5对所有树脂的转化率均表现优异。除了Tetric Ceram树脂,Radii Plus与Ultra - Lume LED 5相当,在Tetric Ceram树脂中Optilux 500表现更优。LEC - 470 I对所有树脂的转化率均较低。
该研究证明了树脂复合材料中不同光引发剂与不同光源兼容性的重要性。