Speziale S, Lonardelli I, Miyagi L, Pehl J, Tommaseo C E, Wenk H-R
Department of Earth and Planetary Science, University of California, Berkeley, CA 94720, USA.
J Phys Condens Matter. 2006 Jun 28;18(25):S1007-20. doi: 10.1088/0953-8984/18/25/S08. Epub 2006 Jun 9.
The combination of the diamond-anvil cell, synchrotron x-ray diffraction in radial geometry and simultaneous Rietveld refinement with texture analysis allows us to quantitatively investigate the plastic deformation behaviour of materials at very high pressures. Our study of copper to 30 GPa shows in ideal experimental geometry a [110] fibre texture component, as is typical for axial compression of soft face centred cubic metals. Locally a plane strain texture develops which is energetically favoured (curling). A transition from compressional to plane strain/pure shear texture can be monitored by analysing individual images taken at different positions in the diamond cell.
金刚石对顶砧室、径向几何同步辐射X射线衍射以及结合织构分析的同时Rietveld精修技术的组合,使我们能够在非常高的压力下定量研究材料的塑性变形行为。我们对高达30吉帕斯卡压力下铜的研究表明,在理想的实验几何条件下,会出现一个[110]纤维织构成分,这是软面心立方金属轴向压缩的典型情况。局部会形成能量上更有利的平面应变织构(卷曲)。通过分析在金刚石对顶砧室不同位置拍摄的单个图像,可以监测从压缩织构到平面应变/纯剪切织构的转变。