N-（4-甲基-苯基-磺酰基）琥珀酰胺酸
N-(4-Methyl-phenyl-sulfon-yl)succinamic acid.
作者信息
Purandara H, Foro Sabine, Gowda B Thimme
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2012 Jun 1;68(Pt 6):o1885. doi: 10.1107/S1600536812023276. Epub 2012 May 26.
Abstract
In the crystal structure of the title compound, C(11)H(13)NO(5)S, the amide C=O and the carboxyl C=O groups of the acid segment orient themselves away from each other. The dihedral angle between the benzene ring and the amide group is 69.0 (2)°. In the crystal, N-H⋯O and O-H⋯O hydrogen bonds link the mol-ecules into layers parallel to the bc plane.
摘要
在标题化合物C₁₁H₁₃NO₅S的晶体结构中，酸片段的酰胺C=O和羧基C=O基团彼此远离排列。苯环与酰胺基团之间的二面角为69.0 (2)°。在晶体中，N-H⋯O和O-H⋯O氢键将分子连接成平行于bc平面的层。
相似文献
1
N-(4-Methyl-phenyl-sulfon-yl)succinamic acid.N-（4-甲基-苯基-磺酰基）琥珀酰胺酸
Acta Crystallogr Sect E Struct Rep Online. 2012 Jun 1;68(Pt 6):o1885. doi: 10.1107/S1600536812023276. Epub 2012 May 26.
2
Crystal structures of three N-(aryl-sulfon-yl)-4-fluoro-benzamides.三种N-（芳基磺酰基）-4-氟苯甲酰胺的晶体结构
Acta Crystallogr E Crystallogr Commun. 2016 Mar 31;72(Pt 4):575-82. doi: 10.1107/S2056989016005089. eCollection 2016 Apr 1.
3
N-(3-Chloro-4-methyl-phen-yl)succinamic acid.N-（3-氯-4-甲基苯基）琥珀酰胺酸
Acta Crystallogr Sect E Struct Rep Online. 2012 Mar 1;68(Pt 3):o835. doi: 10.1107/S1600536812007623. Epub 2012 Feb 24.
4
N-(4-Methyl-phenyl-sulfon-yl)maleamic acid.
Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):o2499. doi: 10.1107/S1600536812032084. Epub 2012 Jul 18.
5
N-(2-Chloro-5-methyl-phen-yl)succinamic acid.N-（2-氯-5-甲基苯基）琥珀酰胺酸
Acta Crystallogr Sect E Struct Rep Online. 2012 Jan;68(Pt 1):o221. doi: 10.1107/S1600536811054638. Epub 2011 Dec 23.
6
2,2-Dichloro-N-(4-chloro-phenyl-sulfon-yl)-acetamide.2,2-二氯-N-(4-氯苯基磺酰基)乙酰胺
Acta Crystallogr Sect E Struct Rep Online. 2008 Jul 19;64(Pt 8):o1521. doi: 10.1107/S1600536808021715.
7
N,N'-Bis(4-methyl-phenyl-sulfon-yl)-suberamide.N,N'-双（4-甲基-苯基-磺酰基）-辛二酰胺
Acta Crystallogr Sect E Struct Rep Online. 2011 Aug 1;67(Pt 8):o2161. doi: 10.1107/S1600536811029783. Epub 2011 Jul 30.
8
N-(4-Chloro-3-methyl-phen-yl)succinamic acid.N-（4-氯-3-甲基苯基）琥珀酰胺酸
Acta Crystallogr Sect E Struct Rep Online. 2012 Jul 1;68(Pt 7):o2003. doi: 10.1107/S1600536812024567. Epub 2012 Jun 13.
9
N-(3-Chloro-2-methyl-phen-yl)succinamic acid.N-（3-氯-2-甲基苯基）琥珀酰胺酸
Acta Crystallogr Sect E Struct Rep Online. 2012 Jun 1;68(Pt 6):o1869. doi: 10.1107/S1600536812022763. Epub 2012 May 23.
10
N-(4-Methyl-2-nitro-phen-yl)succinamic acid.N-（4-甲基-2-硝基苯基）琥珀酰胺酸
Acta Crystallogr Sect E Struct Rep Online. 2012 Mar 1;68(Pt 3):o819. doi: 10.1107/S1600536812007258. Epub 2012 Feb 24.
引用本文的文献
1
N-(4-Methyl-phenyl-sulfon-yl)maleamic acid.
Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):o2499. doi: 10.1107/S1600536812032084. Epub 2012 Jul 18.
本文引用的文献
1
N-(4-Methyl-phen-yl)succinamic acid.N-（4-甲基苯基）琥珀酰胺酸
Acta Crystallogr Sect E Struct Rep Online. 2010 Dec 24;67(Pt 1):o227. doi: 10.1107/S1600536810053298.
2
Structure validation in chemical crystallography.化学晶体学中的结构验证
Acta Crystallogr D Biol Crystallogr. 2009 Feb;65(Pt 2):148-55. doi: 10.1107/S090744490804362X. Epub 2009 Jan 20.
3
Determination of thiocyanate with aromatic halosulphonamides in acid and alkaline media.在酸性和碱性介质中用芳基卤代磺酰胺测定硫氰酸盐。
Talanta. 1983 May;30(5):359-62. doi: 10.1016/0039-9140(83)80080-0.
4
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
Zotero 插件