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Bis(2-amino-3-methyl-pyridine-κN(1))dichloridomercury(II).

作者信息

Tadjarodi Azadeh, Bijanzad Keyvan, Notash Behrouz

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):m1099. doi: 10.1107/S1600536812032126. Epub 2012 Jul 21.

DOI:10.1107/S1600536812032126
PMID:22904756
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3414149/
Abstract

In the title compound, [HgCl(2)(C(6)H(8)N(2))(2)], the two independent Hg(II) cations are each located on a twofold rotation axis and coordinated by two pyridine N atoms from two 2-amino-3-methyl-pyridine ligands and two Cl(-) anions in a distorted tetra-hedral geometry. An intra-molecular N-H⋯Cl hydrogen bond occurs in each independent complex mol-ecule. Inter-molecular N-H⋯Cl hydrogen bonds occur in the crystal structure.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b18d/3414149/765820adda51/e-68-m1099-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b18d/3414149/60de1a034089/e-68-m1099-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b18d/3414149/765820adda51/e-68-m1099-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b18d/3414149/60de1a034089/e-68-m1099-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b18d/3414149/765820adda51/e-68-m1099-fig2.jpg

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本文引用的文献

1
Bis(2-amino-3-methyl-pyridine)-dichlorido-cobalt(II).
Acta Crystallogr Sect E Struct Rep Online. 2010 Sep 25;66(Pt 10):m1293-4. doi: 10.1107/S1600536810036597.
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A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
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High-throughput synthesis and screening of platinum drug candidates.
J Biol Inorg Chem. 2000 Dec;5(6):774-83. doi: 10.1007/s007750000170.