Department of Chemistry, Zakir Husain Delhi College, University of Delhi, J.L.N. Marg, New Delhi 110002, India.
Spectrochim Acta A Mol Biomol Spectrosc. 2012 Nov;97:935-41. doi: 10.1016/j.saa.2012.07.053. Epub 2012 Aug 1.
Benzildiethylenetriamine was used as a reducing agent to prepare Zn nanostructures. The crystallography of benzildiethylenetriamine was done to confirm the molecular structure. These studies focus on the modulation of synthetic parameters in order to influence the size, structure, composition and arrangement of nanoparticles of Zinc. The morphology and structure of the synthesized nanoparticles of zinc were characterized by transmission electron microscopy (TEM), powder X-ray diffraction (XRD), energy dispersive spectrum analysis (EDS), thermal gravimetric analysis (TGA) and infrared spectroscopy (IR). The results show that nanoparticles of zinc are of high purity and 20 nm in size.
苯二亚乙基三胺被用作还原剂来制备 Zn 纳米结构。对苯二亚乙基三胺的晶体学进行了研究，以确认其分子结构。这些研究的重点是调节合成参数，以影响锌纳米粒子的尺寸、结构、组成和排列。通过透射电子显微镜 (TEM)、粉末 X 射线衍射 (XRD)、能谱分析 (EDS)、热重分析 (TGA) 和红外光谱 (IR) 对合成的锌纳米粒子的形貌和结构进行了表征。结果表明，锌纳米粒子的纯度很高，粒径为 20nm。
