Soleimani Hassan, Abbas Zulkifly, Yahya Noorhana, Shameli Kamyar, Soleimani Hojjatollah, Shabanzadeh Parvaneh
Fundamental and Applied Science Department, Universiti Teknologi PETRONAS, Seri Iskandar, 31750, Perak, Malaysia.
Department of Physics, Faculty of Science, Universiti Putra Malaysia, Serdang, 43400 UPM, Selangor, Malaysia.
Int J Mol Sci. 2012;13(7):8540-8548. doi: 10.3390/ijms13078540. Epub 2012 Jul 9.
The sol-gel method was carried out to synthesize nanosized Yttrium Iron Garnet (YIG). The nanomaterials with ferrite structure were heat-treated at different temperatures from 500 to 1000 °C. The phase identification, morphology and functional groups of the prepared samples were characterized by powder X-ray diffraction (PXRD), scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FT-IR), respectively. The YIG ferrite nanopowder was composited with polyvinylidene fluoride (PVDF) by a solution casting method. The magnitudes of reflection and transmission coefficients of PVDF/YIG containing 6, 10 and 13% YIG, respectively, were measured using rectangular waveguide in conjunction with a microwave vector network analyzer (VNA) in X-band frequencies. The results indicate that the presence of YIG in polymer composites causes an increase in reflection coefficient and decrease in transmission coefficient of the polymer.
采用溶胶-凝胶法合成了纳米钇铁石榴石(YIG)。对具有铁氧体结构的纳米材料在500至1000°C的不同温度下进行热处理。分别通过粉末X射线衍射(PXRD)、扫描电子显微镜(SEM)和傅里叶变换红外光谱(FT-IR)对制备样品的相鉴定、形态和官能团进行了表征。通过溶液浇铸法将YIG铁氧体纳米粉末与聚偏氟乙烯(PVDF)复合。分别使用矩形波导结合微波矢量网络分析仪(VNA)在X波段频率下测量了含6%、10%和13% YIG的PVDF/YIG的反射系数和透射系数大小。结果表明,聚合物复合材料中YIG的存在导致聚合物的反射系数增加和透射系数降低。