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通过溶胶-燃烧合成法制备的YFeO细颗粒的尺寸依赖性结构、磁性和磁热性能

Size-Dependent Structural, Magnetic and Magnetothermal Properties of YFeO Fine Particles Obtained by SCS.

作者信息

Kiseleva Tatiana, Abbas Rashad, Martinson Kirill, Komlev Aleksei, Lazareva Evgenia, Tyapkin Pavel, Solodov Evgeniy, Rusakov Vyacheslav, Pyatakov Alexander, Tishin Alexander, Perov Nikolai, Uyanga Enkhnaran, Sangaa Deleg, Popkov Vadim

机构信息

Physics Faculty, Moscow M.V. Lomonosov State University, Leninskie Gory, b.1, Str. 2, 119991 Moscow, Russia.

Saint Petersburg State Institute of Technology, 190013 St. Petersburg, Russia.

出版信息

Nanomaterials (Basel). 2022 Aug 9;12(16):2733. doi: 10.3390/nano12162733.

DOI:10.3390/nano12162733
PMID:36014598
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9415609/
Abstract

Iron-containing oxides are the most important functional substance class and find a tremendous variety of applications. An attractive modern application is their use in biomedical technologies as components in systems for imaging, drug delivery, magnetically mediated hyperthermia, etc. In this paper, we report the results of the experimental investigation of submicron YFeO garnet particles obtained in different sizes by solution combustion synthesis (SCS) using glycine organic fuel to discuss the interdependence of peculiarities of the crystal and magnetic structure and size's influence on its functional magnetothermal performance. A complex study including Mössbauer and Raman spectroscopy accompanied by X-ray diffractometry, SEM, and measurements of field and temperature magnetic properties were performed. The influence of the size effects and perfectness of structure on the particle set magnetization was revealed. The ranges of different mechanisms of magnetothermal effect in the AC magnetic field were determined.

摘要

含铁氧化物是最重要的功能物质类别，有着极为广泛的应用。一个引人注目的现代应用是它们在生物医学技术中作为成像、药物递送、磁介导热疗等系统的组件。在本文中，我们报告了通过使用甘氨酸有机燃料的溶液燃烧合成（SCS）获得的不同尺寸的亚微米YFeO石榴石颗粒的实验研究结果，以讨论晶体和磁结构特性的相互依存关系以及尺寸对其功能磁热性能的影响。进行了一项综合研究，包括穆斯堡尔光谱和拉曼光谱，并辅以X射线衍射、扫描电子显微镜以及场和温度磁性能测量。揭示了尺寸效应和结构完整性对颗粒集合磁化强度的影响。确定了交流磁场中磁热效应不同机制的范围。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/43aa63ef7e76/nanomaterials-12-02733-g011.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/21e97127440a/nanomaterials-12-02733-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/d6cec1600170/nanomaterials-12-02733-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/279b9bafbaee/nanomaterials-12-02733-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/ab48ba742bf8/nanomaterials-12-02733-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/b30e934f5f66/nanomaterials-12-02733-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/f66568799a84/nanomaterials-12-02733-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/43aa63ef7e76/nanomaterials-12-02733-g011.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/15af1f32b9db/nanomaterials-12-02733-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/05b6589695df/nanomaterials-12-02733-g003.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/21e97127440a/nanomaterials-12-02733-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/d6cec1600170/nanomaterials-12-02733-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/279b9bafbaee/nanomaterials-12-02733-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/ab48ba742bf8/nanomaterials-12-02733-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/b30e934f5f66/nanomaterials-12-02733-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/f66568799a84/nanomaterials-12-02733-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c8d/9415609/43aa63ef7e76/nanomaterials-12-02733-g011.jpg

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