• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利：CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法，用中文像聊天一样搜索，搜遍4000万医学文献。AI智能推荐，让科研检索更轻松。

立即免费搜索

文件翻译

保留排版，准确专业，支持PDF/Word/PPT等文件格式，支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述，25分钟生成高质量综述，智能提取关键信息，辅助科研写作。

立即免费体验

2,3-Dibromo-3-(4-chloro-phen-yl)-1-(4-nitro-thio-phen-2-yl)propan-1-one.

作者信息

Fun Hoong-Kun, Arshad Suhana, Shetty Shobhitha, Kalluraya Balakrishna, Babu M

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2012 Sep 1;68(Pt 9):o2681. doi: 10.1107/S1600536812034551. Epub 2012 Aug 11.

DOI:10.1107/S1600536812034551
PMID:22969574
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3435703/
Abstract

The title compound, C(13)H(8)Br(2)ClNO(3)S, exhibits whole-mol-ecule disorder over two orientations in a 0.805 (6):0.195 (6) ratio. The dihedral angles between the thio-phene ring [maximum deviations = 0.017 (4) and 0.033 (9) Å for the major and minor components, respectively] and the chloro-substituted phenyl ring are 32.1 (5) (major component) and 26.3 (18)° (minor component). In the crystal, C-H⋯Cl and C-H⋯O hydrogen bonds link the mol-ecules into sheets lying parallel to the bc plane. Aromatic π-π stacking inter-actions [centroid-centroid distance = 3.550 (7) Å] are also observed.

摘要

相似文献

1
2,3-Dibromo-3-(4-chloro-phen-yl)-1-(4-nitro-thio-phen-2-yl)propan-1-one.
Acta Crystallogr Sect E Struct Rep Online. 2012 Sep 1;68(Pt 9):o2681. doi: 10.1107/S1600536812034551. Epub 2012 Aug 11.
2
Crystal structures of two new carbazole derivatives: 12-(4-nitro-phen-yl)-7-phenyl-sulfonyl-7-benzofuro[2,3-]carbazole and 2-methyl-4-(4-nitro-phen-yl)-9-phenyl-sulfonyl-9-thieno[2,3-]carbazole.两种新型咔唑衍生物的晶体结构：12-(4-硝基苯基)-7-苯基磺酰基-7-苯并呋喃并[2,3-]咔唑和2-甲基-4-(4-硝基苯基)-9-苯基磺酰基-9-噻吩并[2,3-]咔唑。
Acta Crystallogr E Crystallogr Commun. 2016 Nov 4;72(Pt 12):1739-1743. doi: 10.1107/S2056989016016996. eCollection 2016 Dec 1.
3
7-(4-Chloro-benzyl-idene)-3-[(4-chloro-phen-oxy)meth-yl]-6-(4-nitro-thio-phen-2-yl)-7H-1,2,4-triazolo[3,4-b][1,3,4]thia-diazine.7-（4-氯-亚苄基）-3-[(4-氯-苯氧基)甲基]-6-(4-硝基-噻吩-2-基)-7H-1,2,4-三唑并[3,4-b][1,3,4]噻二嗪
Acta Crystallogr Sect E Struct Rep Online. 2011 May 1;67(Pt 5):o1266-7. doi: 10.1107/S1600536811015637. Epub 2011 Apr 29.
4
(E)-3-(2-Chloro-phen-yl)-1-(4-nitro-phen-yl)prop-2-en-1-one.（E）-3-（2-氯苯基）-1-（4-硝基苯基）丙-2-烯-1-酮
Acta Crystallogr Sect E Struct Rep Online. 2008 May 3;64(Pt 6):o958-9. doi: 10.1107/S160053680801218X.
5
(Z)-1-(2-Chloro-phen-yl)-3-methyl-4-[2-(4-nitro-phen-yl)hydrazin-1-yl-idene]-1H-pyrazol-5(4H)-one.（Z）-1-（2-氯苯基）-3-甲基-4-[2-（4-硝基苯基）肼-1-亚基]-1H-吡唑-5（4H）-酮
Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):o2351-2. doi: 10.1107/S1600536812029790. Epub 2012 Jul 7.
6
{2-[(1H-Indol-3-yl-methyl-idene)amino]-4,5,6,7-tetra-hydro-benzo[b]thio-phen-3-yl}(phen-yl)methanone.{2 - [(1H - 吲哚 - 3 - 基亚甲基)氨基] - 4,5,6,7 - 四氢苯并[b]噻吩 - 3 - 基}(苯基)甲酮
Acta Crystallogr Sect E Struct Rep Online. 2014 Mar 29;70(Pt 4):o501-2. doi: 10.1107/S1600536814006345. eCollection 2014 Apr 1.
7
(4-Chloro-phen-yl)[1-(4-methoxy-phen-yl)-3-(5-nitro-2-fur-yl)-1H-pyrazol-4-yl]methanone.（4-氯苯基）[1-（4-甲氧基苯基）-3-（5-硝基-2-呋喃基）-1H-吡唑-4-基]甲酮
Acta Crystallogr Sect E Struct Rep Online. 2010 Apr 14;66(Pt 5):o1063-4. doi: 10.1107/S1600536810011931.
8
2-Anilino-4-(1,3-benzothia-zol-2-yl)-5-(4-chloro-benzo-yl)thio-phene-3-carbonitrile.2-苯胺基-4-(1,3-苯并噻唑-2-基)-5-(4-氯苯甲酰基)噻吩-3-腈
Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):o2529. doi: 10.1107/S1600536812032588. Epub 2012 Jul 25.
9
(1Z,2E)-N'-{1-[2-(4-Bromo-phen-yl)hydrazin-1-yl-idene]-1-chloro-propan-2-yl-idene}thio-phene-2-carbohydrazide.(1Z,2E)-N'-{1-[2-(4-溴苯基)肼-1-亚基]-1-氯丙-2-亚基}噻吩-2-碳酰肼
Acta Crystallogr Sect E Struct Rep Online. 2012 May 1;68(Pt 5):o1510-1. doi: 10.1107/S1600536812017114. Epub 2012 Apr 25.
10
(E)-2-(2,3-Dimethyl-anilino)-N'-(thio-phen-2-yl-methyl-idene)benzohydrazide.（E）-2-（2,3-二甲基苯胺基）-N'-（噻吩-2-基亚甲基）苯甲酰肼
Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):o2524-5. doi: 10.1107/S160053681203259X. Epub 2012 Jul 25.

本文引用的文献

1
2,3-Dibromo-3-(4-chloro-phen-yl)-1-(2-hy-droxy-phen-yl)propan-1-one.2,3-二溴-3-(4-氯苯基)-1-(2-羟基苯基)丙-1-酮
Acta Crystallogr Sect E Struct Rep Online. 2011 Oct 1;67(Pt 10):o2651-2. doi: 10.1107/S1600536811036798. Epub 2011 Sep 17.
2
2,3-Dibromo-1-(4-chloro-phen-yl)-3-(5-nitro-2-fur-yl)propan-1-one.2,3-二溴-1-(4-氯苯基)-3-(5-硝基-2-呋喃基)丙-1-酮
Acta Crystallogr Sect E Struct Rep Online. 2010 Nov 20;66(Pt 12):o3220. doi: 10.1107/S1600536810046829.
3
Structure validation in chemical crystallography.
化学晶体学中的结构验证
Acta Crystallogr D Biol Crystallogr. 2009 Feb;65(Pt 2):148-55. doi: 10.1107/S090744490804362X. Epub 2009 Jan 20.
4
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
5
Convenient access to 1,3,4-trisubstituted pyrazoles carrying 5-nitrothiophene moiety via 1,3-dipolar cycloaddition of sydnones with acetylenic ketones and their antimicrobial evaluation.通过Sydnones与炔酮的1,3-偶极环加成反应便捷合成含5-硝基噻吩部分的1,3,4-三取代吡唑及其抗菌活性评价
Eur J Med Chem. 2008 Aug;43(8):1715-20. doi: 10.1016/j.ejmech.2007.08.002. Epub 2007 Aug 30.