Department of Mechanical Science and Engineering, University of Illinois Urbana-Champaign, Urbana, IL 61801, USA.
Nanotechnology. 2012 Dec 14;23(49):495302. doi: 10.1088/0957-4484/23/49/495302. Epub 2012 Nov 13.
We report a wear-resistant ultrananocrystalline (UNCD) diamond tip integrated onto a heated atomic force microscope (AFM) cantilever and UNCD tips integrated into arrays of heated AFM cantilevers. The UNCD tips are batch-fabricated and have apex radii of approximately 10 nm and heights up to 7 μm. The solid-state heater can reach temperatures above 600 °C and is also a resistive temperature sensor. The tips were shown to be wear resistant throughout 1.2 m of scanning on a single-crystal silicon grating at a force of 200 nN and a speed of 10 μm s(-1). Under the same conditions, a silicon tip was completely blunted. We demonstrate the use of these heated cantilevers for thermal imaging in both contact mode and intermittent contact mode, with a vertical imaging resolution of 1.9 nm. The potential application to nanolithography was also demonstrated, as the tip wrote hundreds of polyethylene nanostructures.
我们报告了一种耐磨的超纳米晶(UNCD)金刚石尖端集成到加热原子力显微镜(AFM)悬臂上,以及 UNCD 尖端集成到加热 AFM 悬臂阵列上。UNCD 尖端是批量制造的,其顶点半径约为 10nm,高度可达 7μm。固态加热器可以达到 600°C 以上的温度,同时也是一个电阻温度传感器。在力为 200nN、速度为 10μm/s 的情况下,这些尖端在对单晶硅光栅进行 1.2m 的扫描过程中表现出了耐磨性能。在相同条件下,硅尖端完全变钝。我们展示了这些加热悬臂在接触模式和间歇接触模式下用于热成像的应用,垂直成像分辨率为 1.9nm。还展示了其在纳米光刻中的潜在应用,因为尖端可以写入数百个聚乙烯纳米结构。