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[Bis[μ-bis-(diphenyl-phosphino)methane-1:2κ(2)P:P']-bis-(nitrito-κ(2)O,O')]disilver(I) acetonitrile disolvate.

作者信息

Yang Xue, Huang Xu, Qiu Qi-Ming, Jin Qiong-Hua, Zhang Cun-Lin

机构信息

Department of Chemistry, Capital Normal University, Beijing 100048, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2012 Nov 1;68(Pt 11):m1367. doi: 10.1107/S1600536812041931. Epub 2012 Oct 13.

DOI:10.1107/S1600536812041931
PMID:23284347
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3515120/
Abstract

The title complex, [Ag(2)(NO(2))(2)(C(25)H(22)P(2))(2)]·2CH(3)CN, is a centrosymmetric dimer in which two bis(diphenylphosphino)methane ligands bridge two Ag(+) ions, forming an eight-membered ring with a short Ag⋯Ag separation of 3.1809 (5) Å. The distorted P(2)O(2) coordination of the cation is completed by two O-donors from a symmetric bidentate chelate NO(2) (-) anion [Ag-O = 2.550 (3) and 2.567 (3) Å].

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/628e/3515120/2c3c70c118f4/e-68-m1367-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/628e/3515120/2c3c70c118f4/e-68-m1367-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/628e/3515120/2c3c70c118f4/e-68-m1367-fig1.jpg

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本文引用的文献

1
(Methanol-κO)(perchlorato-κO)bis-(triphenyl-phosphine-κP)silver(I).
Acta Crystallogr Sect E Struct Rep Online. 2010 Jul 21;66(Pt 8):m969. doi: 10.1107/S160053681002814X.
2
(Perchlorato-κO)tris-(triphenyl-phosphine-κP)silver(I).
Acta Crystallogr Sect E Struct Rep Online. 2010 Jul 3;66(Pt 8):m871. doi: 10.1107/S1600536810025171.
3
catena-Poly[silver(I)-bis-[μ-bis-(diphenyl-phosphino)methane-κP:P']-μ-thio-cyanato-κS:S-silver(I)-μ-thio-cyanato-κS:N].链状聚[银（I）-双-[μ-双-（二苯基膦基）甲烷-κP:P']-μ-硫氰酸根-κS:S-银（I）-μ-硫氰酸根-κS:N]
Acta Crystallogr Sect E Struct Rep Online. 2010 Sep 11;66(Pt 10):m1237-8. doi: 10.1107/S1600536810035622.
4
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.